二环己胺

Mass

MS-NW-5522          
dicyclohexylamine
C12H23N             (Mass of molecular ion:    181)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      27.0       2.8
      28.0       4.1
      29.0       3.9
      30.0       4.4
      39.0       3.5
      41.0      12.6
      42.0       1.8
      43.0       3.5
      44.0       9.1
      53.0       2.0
      54.0       2.7
      55.0      12.5
      56.0      39.2
      57.0       1.9
      67.0       2.6
      68.0       1.9
      69.0       1.4
      70.0       2.7
      79.0       1.1
      81.0       3.1
      82.0       7.7
      83.0       5.0
      96.0       1.9
      98.0       4.9
     100.0       5.5
     110.0       2.7
     124.0       1.5
     125.0       1.6
     138.0     100.0
     139.0      10.9
     152.0       3.2
     180.0       1.1
     181.0      13.9
     182.0       1.9

Assign. Shift(ppm) A 2.546 B 1.856 C 1.712 D 1.606 E 1.246 F 1.146 G 1.021 J 0.7

     Hz     ppm     Int.

   1040.65   2.604     30
   1040.04   2.603     30
   1038.94   2.600     31
   1032.10   2.583    213
   1028.44   2.574    386
   1024.66   2.564    257
   1021.61   2.557    423
   1017.82   2.547    747
   1014.04   2.538    437
   1011.11   2.530    266
   1007.32   2.521    414
   1003.54   2.512    230
    749.15   1.875    758
    746.70   1.869    791
    741.70   1.856    521
    736.57   1.844    811
    735.23   1.840    796
    733.89   1.837    819
    717.16   1.795     46
    715.45   1.791     44
    715.09   1.790     43
    714.72   1.789     43
    694.58   1.738    592
    691.16   1.730    803
    687.62   1.721    646
    681.40   1.705    718
    677.98   1.697    928
    675.54   1.691    706
    662.11   1.657     72
    660.64   1.654     68
    659.18   1.650     64
    658.81   1.649     64
    651.12   1.630    353
    649.41   1.625    400
    648.07   1.622    467
    646.48   1.618    374
    644.65   1.614    347
    639.16   1.600    372
    635.74   1.591    471
    632.20   1.582    341
    628.78   1.574    133
    534.55   1.338     31
    533.81   1.336     31
    530.03   1.327     41
    522.09   1.307    217
    518.80   1.299    310
    515.38   1.290    191
    509.77   1.276    527
    506.47   1.268    816
    503.42   1.260    473
    496.83   1.244    649
    493.77   1.236   1000
    490.97   1.229    614
    484.25   1.212    382
    481.20   1.205    595
    479.00   1.199    387
    474.98   1.189    299
    472.53   1.183    490
    469.60   1.176    306
    463.75   1.161    362
    460.69   1.153    681
    457.28   1.145    372
    451.78   1.131    245
    448.49   1.123    499
    445.07   1.114    262
    439.70   1.101    131
    436.16   1.092    194
    432.62   1.083    138
    426.03   1.067    433
    422.97   1.059    423
    413.33   1.035    865
    411.13   1.029    819
    402.71   1.008    736
    400.15   1.002    790
    390.75   0.978    288
    387.57   0.970    306
    379.15   0.949     33
    377.93   0.946     32
    294.56   0.738     47