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MassMS-NW-3731 cyclohexylamine C6H13N (Mass of molecular ion: 99)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 1.0 18.0 1.2 27.0 3.6 28.0 6.2 29.0 2.5 30.0 8.3 39.0 3.4 41.0 3.5 42.0 4.1 43.0 21.8 44.0 1.2 53.0 1.2 54.0 1.6 55.0 1.9 56.0 100.0 57.0 5.0 67.0 1.4 70.0 6.1 98.0 1.4 99.0 11.4
400 MHz in CDCl3
90 MHz in CDCl3
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1H NMR 399.65 MHz C6 H13 N 0.04 ml : 0.5 ml CDCl3 cyclohexylamine 
Assign. Shift(ppm)
A 2.615 B 1.813 C 1.710 D 1.596 E 1.260 F 1.15 G 1.13 J 1.04 J(A,J)=10.5HZ. J(A,B)=3.9HZ.
Hz ppm Int.1059.57 2.652 250 1055.66 2.642 482 1051.76 2.632 293 1049.07 2.625 496 1045.17 2.616 925 1041.26 2.606 518 1038.45 2.599 281 1034.67 2.589 490 1030.76 2.580 265 735.60 1.841 354 733.03 1.835 603 731.81 1.832 719 730.35 1.828 684 729.25 1.825 709 728.03 1.822 695 726.81 1.819 513 725.34 1.815 469 724.12 1.812 473 722.90 1.809 454 720.21 1.803 646 719.24 1.800 708 718.02 1.797 678 716.43 1.793 715 712.65 1.784 347 697.51 1.746 216 696.66 1.744 223 696.17 1.742 228 693.73 1.736 567 690.06 1.727 746 686.40 1.718 562 685.55 1.716 534 682.74 1.709 399 680.30 1.703 604 676.64 1.694 841 673.22 1.685 577 650.39 1.628 174 648.68 1.624 265 647.22 1.620 378 645.39 1.615 357 643.80 1.611 496 642.33 1.608 327 640.38 1.603 346 638.92 1.599 255 638.31 1.598 243 636.23 1.592 286 634.89 1.589 389 632.69 1.584 333 631.23 1.580 480 630.00 1.577 292 629.64 1.576 296 629.03 1.574 273 627.56 1.571 339 626.22 1.567 211 527.47 1.320 242 523.93 1.311 346 520.51 1.303 205 519.65 1.301 166 515.14 1.289 565 514.28 1.287 463 511.72 1.281 908 510.86 1.279 643 509.16 1.275 388 508.30 1.272 488 507.32 1.270 351 502.81 1.259 545 501.95 1.256 629 499.27 1.250 939 498.54 1.248 922 495.97 1.242 552 489.38 1.225 365 486.21 1.217 609 483.03 1.209 401 468.14 1.172 681 464.97 1.164 1000 461.67 1.156 808 457.40 1.145 512 456.05 1.142 708 452.76 1.133 925 449.10 1.124 478 444.09 1.112 347 440.31 1.102 622 437.01 1.094 349 434.20 1.087 500 431.52 1.080 438 430.66 1.078 453 428.10 1.072 314 422.85 1.059 648 421.63 1.055 757 421.02 1.054 789 419.07 1.049 689 418.33 1.047 697 411.13 1.029 648 410.52 1.028 657 408.45 1.023 647 407.84 1.021 659 398.93 0.999 244 398.19 0.997 229 395.39 0.990 274
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1H NMR 89.56 MHz C6 H13 N 0.04 ml : 0.5 ml CDCl3 cyclohexylamine Assign. Shift(ppm)
A 2.62 B 1.97 to 1.44 C 1.44 to 0.72 D 1.18
Hz ppm Int.235.38 2.629 30 168.06 1.877 50 165.88 1.853 47 165.13 1.844 44 164.19 1.834 49 163.19 1.823 51 162.44 1.814 54 160.31 1.790 58 159.88 1.786 58 157.63 1.761 80 156.50 1.748 82 154.69 1.728 82 153.44 1.714 75 151.94 1.697 68 149.75 1.673 89 148.75 1.661 72 148.19 1.655 68 146.44 1.636 65 144.69 1.616 52 143.31 1.601 42 141.63 1.582 37 118.56 1.324 34 113.63 1.269 39 111.31 1.243 72 108.19 1.209 57 105.31 1.176 1000 97.19 1.086 80 95.63 1.068 59 95.44 1.066 59 92.19 1.030 41
in CDCl3
CCl4 solution
liquid film
4880 A,100M,liquid
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