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网站主页CAS数据库列表 95-00-1更多图谱2,4-二氯苯甲胺(95-00-1)质谱(MS)

2,4-二氯苯甲胺

产品名称 2,4-二氯苯甲胺

CAS号95-00-1

分子式C7H7Cl2N

分子量176.04

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  • Mass

    MS-NW-5645          
    2,4-dichlorobenzylamine
    C7H7Cl2N            (Mass of molecular ion:    175)
    

       Source Temperature: 280 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          28.0      29.0
          29.0      18.6
          30.0      49.5
          36.0       1.3
          37.0       1.7
          38.0       1.7
          39.0       1.6
          49.0       1.1
          50.0       6.3
          50.5       1.6
          51.0       6.3
          51.5      10.1
          52.0       2.9
          61.0       1.5
          62.0       2.2
          63.0       3.0
          69.5       4.3
          70.0       1.0
          70.5       1.4
          73.0       3.3
          74.0       6.2
          75.0      10.1
          76.0       2.3
          77.0      11.5
          78.0       2.1
          84.0       1.5
          85.0       1.9
          86.0       1.2
          87.0       2.4
          88.0       1.1
          89.0       2.5
          99.0       1.1
         100.0       1.3
         102.0       2.5
         104.0       2.4
         109.0       2.4
         110.0       1.0
         111.0      12.6
         112.0       2.4
         113.0       8.2
         114.0       1.1
         115.0       1.4
         123.0       5.2
         124.0       1.5
         125.0       2.0
         136.0       1.4
         138.0       3.7
         139.0       1.1
         140.0     100.0
         141.0       9.3
         142.0      34.6
         143.0       3.0
         146.0       3.3
         147.0       2.8
         148.0       2.5
         149.0       1.8
         159.0      11.0
         160.0       1.2
         161.0       6.6
         163.0       1.2
         172.0       1.3
         174.0      37.6
         175.0       8.9
         176.0      25.2
         177.0       5.5
         178.0       4.2
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C7 H7 Cl2 N 0.04 ml : 0.5 ml CDCl3
    2,4-dichlorobenzylamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.35 B 7.32 C 7.226 D 3.887 E 1.46 J(A,C)=1.8HZ. J(B,C)=8.3HZ.

         Hz     ppm     Int.
    

        664.50   7.420     27
        663.94   7.414     28
        661.50   7.387    235
        661.00   7.381    186
        658.94   7.358    602
        657.13   7.338    686
        653.25   7.294    867
        652.75   7.289    762
        649.56   7.253    910
        647.75   7.233    623
        641.31   7.161    202
        639.50   7.141    150
        348.19   3.888   1000
        342.56   3.825     42
        342.19   3.821     40
        341.13   3.809     30
        130.81   1.461    281
    

in CDCl3



liquid film