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MassMS-IW-1327 p-chloro-N-methylaniline C7H8ClN (Mass of molecular ion: 141)
Source Temperature: 240 °C Sample Temperature: 160 °C Reservoir, 75 eV
28.0 1.5 30.0 1.2 38.0 1.0 39.0 1.4 50.0 3.0 51.0 2.8 52.0 1.9 52.5 1.7 62.0 1.5 63.0 3.6 64.0 1.8 65.0 2.1 70.0 2.9 70.5 3.3 71.0 1.2 71.5 1.0 73.0 2.7 74.0 2.4 75.0 7.2 76.0 1.7 77.0 14.3 78.0 2.1 79.0 1.3 90.0 2.0 91.0 1.7 99.0 7.3 100.0 1.2 101.0 2.4 104.0 5.1 105.0 9.5 106.0 2.8 111.0 6.4 112.0 5.3 113.0 4.5 114.0 1.9 126.0 3.2 127.0 5.2 128.0 1.3 129.0 1.5 138.0 3.2 139.0 1.2 140.0 100.0 141.0 88.8 142.0 38.4 143.0 28.7 144.0 2.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H8 Cl N 0.05 ml : 0.5 ml CDCl3 p-chloro-N-methylaniline 
Assign. Shift(ppm)
A 7.087 B 6.446 C 3. D 2.715
Hz ppm Int.2840.45 7.108 62 2837.16 7.100 478 2834.96 7.094 178 2833.01 7.089 24 2832.28 7.087 24 2830.44 7.083 185 2828.25 7.077 486 2824.95 7.069 76 2583.98 6.466 60 2580.69 6.458 445 2578.49 6.452 160 2573.97 6.441 155 2571.78 6.436 413 2568.48 6.427 59 1433.96 3.589 20 1085.08 2.716 1000
in CDCl3
liquid film
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