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网站主页CAS数据库列表 929-59-9更多图谱1,8-二氨基-3,6-二氧杂辛烷(929-59-9)核磁图(1HNMR)

1,8-二氨基-3,6-二氧杂辛烷

产品名称 1,8-二氨基-3,6-二氧杂辛烷

CAS号929-59-9

分子式C6H16N2O2

分子量148.2

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  • Mass

    MS-IW-9153          
    2,2'-(ethylenedioxy)diethylamine
    C6H16N2O2           (Mass of molecular ion:    148)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       2.9
          17.0       1.3
          18.0      18.1
          27.0       4.6
          28.0      12.2
          29.0       4.5
          30.0     100.0
          31.0      14.9
          41.0       2.9
          42.0      11.0
          43.0      22.1
          44.0      59.3
          45.0       9.2
          55.0       1.3
          56.0       4.8
          57.0       3.5
          58.0       4.5
          59.0       2.4
          60.0       3.6
          61.0      29.1
          62.0       3.5
          68.0       2.7
          69.0       6.6
          70.0       1.5
          72.0      12.0
          73.0       1.1
          74.0       1.3
          81.0       1.1
          84.0       1.7
          86.0       1.2
          87.0       7.1
          88.0       1.6
          89.0      26.7
          90.0       1.3
         102.0       3.8
         106.0       6.4
         119.0      24.6
         120.0       1.5
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C6 H16 N2 O2 0.05 ml : 0.5 ml CDCl3
    2,2'-(ethylenedioxy)diethylamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.635 B 3.514 C 2.866 D 1.28

         Hz     ppm     Int.
    

       1452.88   3.636   1000
       1409.79   3.528    363
       1404.54   3.515    486
       1399.29   3.502    365
       1150.63   2.880    130
       1145.63   2.867    182
       1140.63   2.855    116
        509.77   1.276     96
    

in CDCl3



liquid film