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MassMS-NW-8491 N-ethyl-N-phenylbenzylamine C15H17N (Mass of molecular ion: 211)
Source Temperature: 260 °C Sample Temperature: 140 °C Reservoir, 75 eV
27.0 1.8 28.0 1.2 29.0 1.8 39.0 4.3 41.0 1.4 50.0 1.2 51.0 7.3 52.0 1.3 63.0 2.0 64.0 1.0 65.0 11.0 77.0 16.5 78.0 2.4 79.0 1.7 89.0 1.5 91.0 100.0 92.0 8.5 104.0 5.8 105.0 2.0 106.0 4.6 118.0 1.2 120.0 1.7 134.0 7.6 180.0 1.6 182.0 1.2 196.0 17.0 197.0 2.7 210.0 1.6 211.0 22.7 212.0 3.9
400 MHz in CDCl3
90 MHz in CDCl3
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1H NMR 399.65 MHz C15 H17 N 0.05 ml : 0.5 ml CDCl3 N-ethyl-N-phenylbenzylamine 
Assign. Shift(ppm)
A 7.258 B 7.207 C 7.18 D 7.15 E 6.66 F 6.64 G 4.461 J 3.418 K 1.159
Hz ppm Int.2909.91 7.282 97 2908.81 7.279 138 2907.35 7.275 69 2902.34 7.263 247 2901.49 7.261 329 2900.51 7.258 249 2896.36 7.248 134 2894.41 7.243 380 2883.30 7.215 418 2876.34 7.198 298 2871.46 7.185 87 2869.38 7.180 190 2865.72 7.171 157 2864.01 7.167 141 2862.18 7.162 93 2861.57 7.161 97 2859.01 7.154 348 2857.30 7.150 367 2854.98 7.144 67 2852.17 7.137 115 2850.10 7.132 312 2847.66 7.126 49 2669.68 6.681 294 2668.70 6.678 396 2661.74 6.661 284 2660.77 6.658 445 2659.79 6.656 374 2657.35 6.650 61 2654.54 6.643 168 2653.56 6.640 253 2647.22 6.624 83 2646.24 6.622 124 2645.39 6.620 70 1783.08 4.462 674 1376.71 3.445 148 1369.63 3.428 419 1362.55 3.410 420 1355.47 3.392 149 470.46 1.178 556 463.38 1.160 1000 459.47 1.150 41 456.30 1.142 533
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1H NMR 89.56 MHz C15 H17 N 0.04 ml : 0.5 ml CDCl3 N-ethyl-N-phenylbenzylamine Assign. Shift(ppm)
A 7.25 B 7.16 C 6.76 D 6.65 E 4.495 F 3.434 G 1.186
Hz ppm Int.652.38 7.285 79 652.25 7.283 79 651.81 7.278 80 650.88 7.268 163 649.00 7.247 1000 645.50 7.208 89 643.63 7.187 118 642.06 7.170 150 641.38 7.162 226 639.38 7.140 39 637.31 7.117 51 634.38 7.084 172 605.25 6.759 35 602.44 6.727 304 600.13 6.701 61 595.31 6.648 181 594.69 6.641 187 593.63 6.629 129 589.19 6.579 31 588.00 6.566 47 402.63 4.496 410 319.69 3.570 60 312.63 3.491 194 305.63 3.413 208 298.50 3.333 72 113.06 1.263 290 106.06 1.185 583 99.00 1.106 248
in CDCl3
CCl4 solution
liquid film
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