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MS-NW-3811 ethyl p-hydroxybenzoate C9H10O3 (Mass of molecular ion: 166)
Source Temperature: 270 °C Sample Temperature: 180 °C Reservoir, 75 eV
27.0 4.4 29.0 4.0 38.0 2.1 39.0 11.5 50.0 1.0 53.0 1.7 62.0 1.2 63.0 3.5 64.0 2.5 65.0 16.9 66.0 1.5 92.0 2.3 93.0 15.0 94.0 2.0 109.0 1.0 121.0 100.0 122.0 11.5 123.0 1.1 138.0 21.2 139.0 1.8 151.0 1.5 166.0 23.2 167.0 2.5
90 MHz in CDCl3
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1H NMR 89.56 MHz C9 H10 O3 0.057 g : 0.5 ml CDCl3 ethyl p-hydroxybenzoate Assign. Shift(ppm)
A 7.954 B 7.70 C 6.926 D 4.364 E 1.386
Hz ppm Int.
719.75 8.037 65 717.13 8.008 441 715.00 7.984 135 710.38 7.932 168 708.19 7.908 503 705.63 7.879 68 690.00 7.705 390 627.13 7.003 74 624.44 6.973 525 622.31 6.949 148 617.63 6.897 147 615.50 6.873 427 612.75 6.842 59 402.06 4.490 121 401.94 4.488 121 394.81 4.409 424 387.69 4.329 446 380.63 4.251 145 131.13 1.465 463 128.06 1.430 50 127.75 1.427 50 127.25 1.421 53 124.06 1.386 1000 121.69 1.359 63 119.38 1.333 51 116.88 1.306 418
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