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MS-NW-6154 1-naphthol C10H8O (Mass of molecular ion: 144)
Source Temperature: 250 °C Sample Temperature: 190 °C Reservoir, 75 eV
38.0 1.2 39.0 3.8 50.0 2.4 51.0 2.7 57.0 3.7 57.5 4.7 58.0 5.6 61.0 1.1 62.0 3.0 63.0 6.3 64.0 1.3 65.0 2.7 72.0 5.9 74.0 2.2 75.0 1.9 77.0 1.0 86.0 1.3 87.0 1.8 88.0 1.7 89.0 6.0 90.0 1.3 113.0 1.6 114.0 2.8 115.0 56.1 116.0 30.6 117.0 2.9 143.0 1.5 144.0 100.0 145.0 11.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H8 O 0.039 g : 0.5 ml CDCl3 1-naphthol Assign. Shift(ppm)
A 8.161 B 7.786 C 7.47 D 7.45 E 7.417 F 7.259 G 6.734 J 5.43
Hz ppm Int.
3269.41 8.181 74 3268.55 8.179 90 3267.21 8.176 254 3266.48 8.174 403 3265.75 8.172 283 3265.14 8.171 251 3264.16 8.168 214 3262.08 8.163 198 3261.23 8.161 342 3260.62 8.159 279 3259.77 8.157 253 3259.03 8.155 242 3257.57 8.152 274 3256.84 8.150 422 3256.10 8.148 249 3120.85 7.809 78 3120.48 7.809 79 3117.31 7.801 389 3114.99 7.795 298 3113.16 7.790 376 3109.74 7.782 284 3109.38 7.781 296 3107.79 7.777 439 3105.35 7.771 79 2992.80 7.489 95 2990.60 7.484 231 2985.96 7.472 804 2984.74 7.469 832 2983.76 7.466 665 2980.83 7.459 917 2980.35 7.458 867 2977.17 7.450 654 2976.44 7.448 724 2975.10 7.445 701 2973.51 7.441 111 2970.21 7.433 473 2969.24 7.430 579 2961.91 7.412 428 2960.94 7.409 700 2960.57 7.408 649 2908.57 7.278 759 2901.12 7.260 880 2900.39 7.258 661 2892.94 7.239 615 2695.56 6.745 761 2694.58 6.743 736 2688.11 6.727 707 2687.13 6.724 674 2170.53 5.432 1000
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