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MassMS-NW-1515 2-naphthol C10H8O (Mass of molecular ion: 144)
Source Temperature: 250 °C Sample Temperature: 170 °C Reservoir, 75 eV
27.0 1.2 38.0 2.3 39.0 6.3 50.0 4.4 51.0 4.9 53.0 1.1 57.0 1.6 57.5 2.5 58.0 1.8 61.0 1.9 62.0 5.7 63.0 11.0 64.0 2.0 65.0 4.4 72.0 3.2 74.0 3.5 75.0 2.9 76.0 1.4 77.0 1.1 86.0 2.1 87.0 3.5 88.0 2.8 89.0 10.8 90.0 1.5 113.0 2.6 114.0 3.9 115.0 70.7 116.0 24.1 117.0 1.9 126.0 1.2 143.0 1.3 144.0 100.0 145.0 10.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H8 O 20.1 mg : 0.5 ml CDCl3 2-naphthol 
Assign. Shift(ppm)
A 7.75 B 7.74 C 7.655 D 7.417 E 7.321 F 7.122 G 7.089 J 5.19 J(F,G)=2.6HZ. J(B,G)=8.6HZ.
Hz ppm Int.3104.61 7.769 391 3104.13 7.768 374 3096.44 7.748 903 3095.70 7.747 1000 3091.67 7.736 66 3087.16 7.725 582 3064.33 7.668 391 3063.60 7.666 362 3056.03 7.647 470 3055.30 7.645 437 2972.66 7.439 237 2971.31 7.435 239 2965.70 7.421 358 2964.48 7.418 468 2963.13 7.415 223 2957.52 7.401 296 2956.30 7.398 264 2933.47 7.341 357 2932.25 7.338 348 2926.76 7.324 289 2925.42 7.320 530 2924.07 7.317 329 2918.46 7.303 249 2917.24 7.300 224 2848.14 7.127 496 2845.70 7.121 716 2838.50 7.103 637 2835.94 7.097 383 2829.83 7.081 539 2827.27 7.075 406
in CDCl3
CCl4 solution
KBr disc
nujol mull
OXIDATION WITH CERIC SULPHATE IN H2SO4
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