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MS-NW-0827 1-decene C10H20 (Mass of molecular ion: 140)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 23.5 28.0 5.1 29.0 37.5 39.0 25.0 40.0 4.0 41.0 83.5 42.0 35.0 43.0 81.5 44.0 2.7 51.0 1.6 53.0 7.2 54.0 11.8 55.0 87.7 56.0 100.0 57.0 69.3 58.0 3.0 65.0 1.1 67.0 8.3 68.0 9.8 69.0 57.3 70.0 80.7 71.0 12.5 81.0 1.9 82.0 7.0 83.0 33.7 84.0 24.9 85.0 5.7 96.0 2.7 97.0 21.7 98.0 15.2 99.0 1.4 111.0 10.1 112.0 7.2 140.0 11.9 141.0 1.4
90 MHz in CDCl3
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1H NMR 89.56 MHz C10 H20 0.04 ml : 0.5 ml CDCl3 1-decene Assign. Shift(ppm)
A 5.79 B 4.98 C 4.92 D 2.03 E 1.41 F 1.28 G 0.89
Hz ppm Int.
535.06 5.975 51 525.13 5.864 64 524.38 5.856 45 518.69 5.792 39 517.88 5.783 83 514.38 5.744 45 511.31 5.710 46 507.94 5.672 98 501.50 5.600 55 457.00 5.103 38 455.56 5.087 83 454.63 5.077 84 454.06 5.070 62 453.19 5.061 155 451.75 5.045 77 447.50 4.997 67 446.31 4.984 136 445.13 4.971 104 443.94 4.957 76 442.81 4.945 39 438.38 4.895 47 437.44 4.885 78 436.38 4.873 148 436.00 4.869 146 435.19 4.860 104 434.56 4.853 84 434.06 4.847 62 185.63 2.073 71 184.94 2.065 68 179.25 2.002 84 174.88 1.953 35 174.31 1.947 36 173.75 1.941 38 173.25 1.935 38 172.75 1.929 38 130.13 1.453 45 129.63 1.448 46 125.88 1.406 71 125.38 1.400 72 114.94 1.284 1000 103.69 1.158 38 101.81 1.137 30 83.94 0.938 103 81.63 0.912 84 80.94 0.904 86 78.94 0.882 321 72.81 0.813 66
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