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MassMS-NW-5549 cis-9-octadecen-1-ol C18H36O (Mass of molecular ion: 268)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
18.0 2.3 27.0 9.4 28.0 3.9 29.0 23.6 31.0 11.0 39.0 8.1 40.0 1.8 41.0 63.7 42.0 11.6 43.0 51.3 44.0 2.1 45.0 1.7 53.0 6.4 54.0 35.6 55.0 100.0 56.0 27.2 57.0 35.3 58.0 1.8 65.0 1.7 66.0 5.6 67.0 60.2 68.0 49.7 69.0 64.7 70.0 21.2 71.0 13.9 72.0 1.2 77.0 1.7 79.0 5.9 80.0 5.3 81.0 56.7 82.0 82.7 83.0 50.6 84.0 11.7 85.0 7.7 91.0 1.5 93.0 2.6 94.0 3.0 95.0 46.8 96.0 59.8 97.0 30.9 98.0 7.2 99.0 1.9 107.0 1.3 108.0 1.5 109.0 25.1 110.0 23.0 111.0 12.1 112.0 3.7 113.0 1.0 121.0 1.5 122.0 1.1 123.0 12.8 124.0 13.4 125.0 4.9 126.0 2.2 135.0 1.0 137.0 6.8 138.0 7.4 139.0 1.9 140.0 1.3 151.0 2.8 152.0 3.9 153.0 1.0 165.0 1.6 166.0 2.6 180.0 1.7 194.0 1.7 208.0 1.0 222.0 2.0 250.0 6.3 251.0 1.3
90 MHz in CDCl3
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1H NMR 89.56 MHz C18 H36 O 0.04 ml : 0.5 ml CDCl3 cis-9-octadecen-1-ol 
Assign. Shift(ppm)
A *1 5.35 B *1 5.34 C 3.629 D 2.00 E 1.57 F 1.45 to 1.23 G 0.881
Hz ppm Int.484.44 5.410 50 483.38 5.398 73 480.13 5.361 69 478.81 5.347 163 477.69 5.334 68 474.38 5.297 68 473.31 5.285 55 331.81 3.705 64 325.56 3.636 189 319.25 3.565 95 183.06 2.044 88 182.31 2.036 86 178.44 1.993 95 177.88 1.987 97 177.25 1.980 96 117.25 1.310 777 113.31 1.266 1000 78.94 0.882 215 72.94 0.815 49
in CDCl3
CCl4 solution
liquid film
4880 A,100M,liquid
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