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3,6-二氨基咔唑

产品名称 3,6-二氨基咔唑

CAS号86-71-5

分子式C12H11N3

分子量197.24

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  • Mass

    MS-IW-3665          
    3,6-carbazolediamine
    C12H11N3            (Mass of molecular ion:    197)
    

       Source Temperature: 140 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          17.0       1.4
          18.0       7.1
          28.0       1.4
          52.0       1.2
          63.0       1.5
          70.5       2.9
          71.0       1.2
          71.5       2.0
          84.0       1.4
          84.5       7.7
          85.0       3.2
          89.0       1.7
          90.0       1.4
          98.0       5.0
          98.5      13.6
          99.0       2.0
         114.0       1.2
         115.0       2.8
         116.0       1.6
         140.0       2.1
         141.0       1.7
         142.0       1.9
         143.0       2.6
         144.0       1.0
         145.0       1.2
         152.0       2.0
         153.0       1.4
         154.0       1.1
         168.0       3.5
         169.0       8.5
         170.0       2.4
         179.0       2.7
         180.0       2.4
         181.0       5.9
         194.0       1.2
         195.0       1.5
         196.0      33.5
         197.0     100.0
         198.0      13.9
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C12 H11 N3 0.035 g : 0.5 ml DMSO-d6
    3,6-carbazolediamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 10.07 B 7.081 C 7.077 D 6.688 E 4.51

         Hz     ppm     Int.
    

       4023.59  10.068    331
       2834.01   7.092    737
       2829.90   7.081    701
       2827.45   7.075    760
       2825.93   7.072    895
       2815.55   7.046     22
       2678.07   6.702    449
       2675.93   6.696    444
       2669.53   6.680    396
       2667.39   6.675    427
       1803.13   4.512   1000
    

in DMSO-d6



KBr disc



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