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MassMS-IW-3665 3,6-carbazolediamine C12H11N3 (Mass of molecular ion: 197)
Source Temperature: 140 °C Sample Temperature: 120 °C Direct, 75 eV
17.0 1.4 18.0 7.1 28.0 1.4 52.0 1.2 63.0 1.5 70.5 2.9 71.0 1.2 71.5 2.0 84.0 1.4 84.5 7.7 85.0 3.2 89.0 1.7 90.0 1.4 98.0 5.0 98.5 13.6 99.0 2.0 114.0 1.2 115.0 2.8 116.0 1.6 140.0 2.1 141.0 1.7 142.0 1.9 143.0 2.6 144.0 1.0 145.0 1.2 152.0 2.0 153.0 1.4 154.0 1.1 168.0 3.5 169.0 8.5 170.0 2.4 179.0 2.7 180.0 2.4 181.0 5.9 194.0 1.2 195.0 1.5 196.0 33.5 197.0 100.0 198.0 13.9
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C12 H11 N3 0.035 g : 0.5 ml DMSO-d6 3,6-carbazolediamine 
Assign. Shift(ppm)
A 10.07 B 7.081 C 7.077 D 6.688 E 4.51
Hz ppm Int.4023.59 10.068 331 2834.01 7.092 737 2829.90 7.081 701 2827.45 7.075 760 2825.93 7.072 895 2815.55 7.046 22 2678.07 6.702 449 2675.93 6.696 444 2669.53 6.680 396 2667.39 6.675 427 1803.13 4.512 1000
in DMSO-d6
KBr disc
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