图谱信息 供应商 相关产品
网站主页CAS数据库列表 85006-21-9更多图谱2-氯-5-甲氧基苯胺盐酸盐(85006-21-9)核磁图(1HNMR)

2-氯-5-甲氧基苯胺盐酸盐

产品名称 2-氯-5-甲氧基苯胺盐酸盐

CAS号85006-21-9

分子式C7H9Cl2NO

分子量194.06

展开


  • Mass

    MS-KW-0182          
    6-chloro-m-anisidine hydrochloride
    C7H8ClNO HCl        (Mass of molecular ion:    157)
    

       Source Temperature: 170 °C
       Sample Temperature: 140 °C
       Direct, 75 eV
    

          18.0       3.6
          28.0       3.2
          35.0       2.6
          36.0      36.7
          37.0       1.6
          38.0      13.3
          39.0       2.9
          41.0       1.7
          46.5       1.7
          50.0       1.8
          51.0       7.1
          52.0       5.9
          53.0       1.8
          61.0       1.6
          62.0       2.3
          63.0       4.7
          64.0       2.1
          65.0       4.1
          68.0       1.2
          73.0       2.1
          75.0       1.3
          76.0       1.1
          77.0       1.3
          78.0       6.4
          78.5       4.0
          79.0       3.7
          79.5       1.3
          87.0       2.9
          89.0       1.4
          90.0       4.2
          91.0       2.2
          92.0       5.1
          93.0      12.2
          94.0       9.3
          95.0       1.3
          99.0       1.7
         100.0       1.4
         106.0       1.0
         114.0      22.3
         115.0       1.6
         116.0       7.4
         122.0       2.0
         126.0       1.7
         127.0      20.2
         128.0      21.2
         129.0      12.2
         130.0       7.2
         131.0       2.1
         142.0       1.5
         156.0       5.7
         157.0     100.0
         158.0       9.9
         159.0      31.8
         160.0       2.6
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C7 H8 Cl N O 0.037 g : 0.5 ml DMSO-d6
    6-chloro-m-anisidine hydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.65 B 7.374 C 7.081 D 6.738 E 3.744

         Hz     ppm     Int.
    

       3857.73   9.653     83
       2951.66   7.386    192
       2942.81   7.364    206
       2831.42   7.085    147
       2828.37   7.078    149
       2698.52   6.753     91
       2695.62   6.745     87
       2689.67   6.731     85
       2686.77   6.723     80
       1496.43   3.745   1000
    

in DMSO-d6



KBr disk



Nujol