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网站主页CAS数据库列表 85-83-6更多图谱溶剂红 24(85-83-6)核磁图(13CNMR)

溶剂红 24

产品名称 溶剂红 24

CAS号85-83-6

分子式C24H20N4O

分子量380.44

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  • Mass

    MS-NW-6642          
    Sudan IV
    C24H20N4O           (Mass of molecular ion:    380)
    

       Source Temperature: 220 °C
       Sample Temperature: 170 °C
       Direct, 75 eV
    

          18.0       2.4
          27.0       1.5
          28.0       2.0
          39.0       7.3
          41.0       2.6
          50.0       1.9
          51.0       6.9
          52.0       3.2
          53.0       1.4
          62.0       1.1
          63.0       5.8
          64.0       2.7
          65.0      18.6
          66.0       1.7
          75.0       2.7
          76.0       2.7
          77.0      11.3
          78.0       5.0
          79.0       3.2
          88.0       1.4
          89.0      11.9
          90.0       9.3
          91.0      75.3
          92.0       7.3
          93.0       1.3
         101.0       4.7
         102.0       3.8
         103.0       2.2
         104.0       8.1
         105.0       3.4
         106.0      12.7
         107.0       3.2
         113.0       1.2
         114.0       4.5
         115.0      39.2
         116.0       4.5
         118.0       1.3
         119.0      10.7
         120.0       1.2
         121.0       1.2
         127.0       1.3
         128.0       7.4
         129.0       6.0
         130.0       3.3
         134.0       1.7
         142.0       1.7
         143.0      57.7
         144.0       9.5
         145.0       1.0
         152.0       1.0
         156.0       2.5
         157.0       1.4
         158.0       2.5
         159.0       2.0
         165.0       3.4
         166.0       1.4
         167.0       1.1
         170.0       4.4
         171.0      16.6
         172.0       2.1
         178.0       1.2
         179.0       1.2
         180.0       2.8
         181.0       2.0
         182.0       1.0
         189.0       1.9
         190.0       4.9
         190.5       1.0
         194.0       2.3
         195.0       3.0
         196.0       1.9
         197.0       2.1
         202.0       1.2
         203.0       1.2
         204.0       1.3
         205.0       1.9
         206.0       1.4
         207.0       1.9
         208.0       2.7
         209.0       4.6
         210.0       2.5
         215.0       1.4
         216.0       1.5
         217.0       1.6
         218.0       4.1
         219.0       2.0
         220.0       1.2
         222.0       2.9
         223.0       8.3
         224.0       8.7
         225.0       6.0
         226.0       1.2
         230.0       1.7
         231.0       2.4
         232.0       4.8
         233.0       7.9
         234.0       2.6
         244.0       4.1
         245.0       2.2
         246.0       2.3
         247.0       1.0
         259.0       1.1
         260.0       2.2
         261.0      77.8
         262.0      15.1
         263.0       1.7
         275.0       1.1
         277.0       1.3
         289.0       1.1
         349.0       2.4
         350.0       1.1
         351.0       2.8
         352.0       2.6
         363.0       2.3
         379.0       2.6
         380.0     100.0
         381.0      28.2
         382.0       4.2
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C24 H20 N4 O 0.033 g : 0.5 ml CDCl3
    Sudan IV
    ChemicalStructure
        Assign.     Shift(ppm)
    A 16.53 B 8.463 C 8.103 D 7.879 E 7.750 F 7.62 J 7.518 K 7.486 L 7.35 M 7.34 N 7.31 P 7.26 Q 6.748 R 2.718 S 2.535 ASSIGNED BY H-H AND C-H COSY. J(F,Q)=9.5HZ

         Hz     ppm     Int.
    

       6606.93  16.532    147
       3386.72   8.475    124
       3378.66   8.455    131
       3243.41   8.116    150
       3234.86   8.095    180
       3153.81   7.892    104
       3152.10   7.888    106
       3145.02   7.870     87
       3143.31   7.866     90
       3097.90   7.752    190
       3096.92   7.750    180
       3048.58   7.629    208
       3042.24   7.613    165
       3038.82   7.604    183
       3011.96   7.537     70
       3004.88   7.519    129
       2996.34   7.498    154
       2988.04   7.477    146
       2946.29   7.373     97
       2945.56   7.371    102
       2938.48   7.353    154
       2934.33   7.343    130
       2933.11   7.340    136
       2931.64   7.336    117
       2927.98   7.327    302
       2927.00   7.324    296
       2920.65   7.309     59
       2906.74   7.274     78
       2904.54   7.268     72
       2898.44   7.253    104
       2892.58   7.238     47
       2890.38   7.233     42
       2701.90   6.761    207
       2692.38   6.737    196
       1094.48   2.739     40
       1093.99   2.738     40
       1086.67   2.720   1000
       1013.43   2.536    862
    

in CDCl3



KBr disc



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