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MassMS-NW-3899 benzo(f)quinoline C13H9N (Mass of molecular ion: 179)
Source Temperature: 270 °C Sample Temperature: 180 °C Reservoir, 75 eV
50.0 1.6 51.0 1.5 62.0 1.3 63.0 3.6 74.0 1.9 75.0 3.6 75.5 2.1 76.0 7.7 89.0 1.5 89.5 3.7 125.0 1.0 126.0 2.7 150.0 4.5 151.0 10.8 152.0 8.9 153.0 2.7 177.0 4.1 178.0 18.4 179.0 100.0 180.0 14.8 181.0 1.0
400 MHz in CDCl3
90 MHz in CDCl3
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1H NMR 399.65 MHz C13 H9 N 12.9 mg : 0.5 ml CDCl3 benzo(f)quinoline 
Assign. Shift(ppm)
A 8.97 B 8.95 C 8.620 D 7.996 E 7.990 F 7.939 G *1 7.697 J *1 7.659 K 7.557
Hz ppm Int.3586.79 8.975 185 3585.21 8.971 270 3582.40 8.964 224 3580.81 8.960 457 3578.74 8.955 208 3576.05 8.948 34 3575.68 8.948 34 3575.32 8.947 34 3574.71 8.945 32 3572.02 8.938 275 3570.31 8.934 204 3449.71 8.632 206 3449.22 8.631 214 3448.36 8.629 226 3441.04 8.611 220 3440.43 8.609 232 3204.22 8.018 77 3198.00 8.003 31 3195.07 7.995 988 3194.58 7.994 1000 3193.73 7.992 994 3189.58 7.981 43 3188.96 7.980 37 3188.60 7.979 32 3188.11 7.978 30 3187.87 7.977 30 3186.52 7.974 30 3184.45 7.969 79 3178.10 7.953 223 3177.61 7.951 222 3176.64 7.949 224 3175.78 7.947 192 3173.58 7.941 32 3172.24 7.938 30 3170.29 7.933 304 3168.82 7.929 273 3085.69 7.721 129 3084.11 7.718 150 3078.61 7.704 304 3077.03 7.700 278 3075.93 7.697 153 3074.71 7.694 37 3074.34 7.693 30 3070.68 7.684 320 3068.97 7.680 283 3067.14 7.675 310 3065.55 7.671 340 3063.35 7.666 31 3060.06 7.657 200 3059.33 7.656 280 3057.98 7.652 278 3052.25 7.638 140 3050.90 7.634 118 3026.61 7.574 376 3022.22 7.563 367 3018.31 7.553 369 3013.92 7.542 367
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1H NMR 89.56 MHz C13 H9 N 0.045 g : 0.5 ml CDCl3 benzo[f]quinoline Assign. Shift(ppm)
A 8.93 B 8.86 C 8.53 D 7.95 E 8.07 to 7.48 F 7.482
Hz ppm Int.802.81 8.964 199 801.13 8.946 354 798.31 8.914 321 797.63 8.907 295 796.75 8.897 412 789.25 8.813 245 787.63 8.795 169 769.50 8.593 123 769.13 8.588 129 766.69 8.561 90 764.94 8.542 132 761.81 8.507 102 759.63 8.482 159 712.63 7.958 746 712.06 7.951 1000 708.63 7.913 148 706.00 7.883 161 704.50 7.867 158 701.75 7.836 256 701.13 7.829 227 698.25 7.797 60 691.50 7.722 103 687.19 7.673 394 686.00 7.660 388 684.50 7.643 235 682.31 7.619 380 681.38 7.609 357 679.19 7.584 217 676.94 7.559 314 675.81 7.546 393 671.38 7.497 355 667.44 7.453 331 663.00 7.403 315
in CDCl3
KBr disc
nujol mull
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