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网站主页CAS数据库列表 229-87-8更多图谱菲啶(229-87-8)Raman光谱

菲啶

产品名称 菲啶

CAS号229-87-8

分子式C13H9N

分子量179.22

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  • Mass

    MS-NW-8646          
    phenanthridine
    C13H9N              (Mass of molecular ion:    179)
    

       Source Temperature: 260 °C
       Sample Temperature: 140 °C
       Reservoir, 75 eV
    

          17.0       1.0
          18.0       5.4
          39.0       1.3
          50.0       1.7
          51.0       1.9
          62.0       1.4
          63.0       5.9
          74.0       1.9
          75.0       4.4
          75.5       2.6
          76.0      11.0
          76.5       1.5
          77.0       1.2
          87.0       1.0
          89.0       2.2
          89.5       5.6
          99.0       1.1
         125.0       1.3
         126.0       2.5
         127.0       1.1
         150.0       4.8
         151.0      11.3
         152.0       8.9
         153.0       4.4
         177.0       4.5
         178.0      17.1
         179.0     100.0
         180.0      14.4
         181.0       1.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C13 H9 N 0.036 g : 0.5 ml CDCl3
    phenanthridine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.256 B 8.537 C 8.517 D 8.188 E 7.987 F 7.880 G 7.723 J 7.65 K 7.64 ASSIGNED BY C-H COSY

         Hz     ppm     Int.
    

       3699.49   9.257    768
       3416.29   8.549    520
       3407.59   8.527   1000
       3400.73   8.510    497
       3399.35   8.506    500
       3277.28   8.201    468
       3276.06   8.198    493
       3269.04   8.180    515
       3267.97   8.178    530
       3196.72   7.999    458
       3196.11   7.998    476
       3188.78   7.979    520
       3188.17   7.978    535
       3126.22   7.823    298
       3124.85   7.819    308
       3119.05   7.805    420
       3117.83   7.802    640
       3116.61   7.799    346
       3110.81   7.784    379
       3109.44   7.781    365
       3095.70   7.747    266
       3094.18   7.743    284
       3088.68   7.729    446
       3087.31   7.726    571
       3086.09   7.722    320
       3080.60   7.709    401
       3079.07   7.705    394
       3066.71   7.674    426
       3065.64   7.671    451
       3063.20   7.665    412
       3061.68   7.661    436
       3058.78   7.654    705
       3057.86   7.652    516
       3056.03   7.647    352
       3054.81   7.644    594
       3053.59   7.641    445
       3051.76   7.637    343
       3050.69   7.634    336
       3047.94   7.627    267
       3046.57   7.624    256
    

in CDCl3



KBr disc



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