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网站主页CAS数据库列表 836-30-6更多图谱4-硝基二苯胺(836-30-6)Raman光谱

4-硝基二苯胺

产品名称 4-硝基二苯胺

CAS号836-30-6

分子式C12H10N2O2

分子量214.22

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  • Mass

    MS-NW-1765          
    4-nitrodiphenylamine
    C12H10N2O2          (Mass of molecular ion:    214)
    

       Source Temperature: 180 °C
       Sample Temperature: 160 °C
       Direct, 75 eV
    

          27.0       1.5
          28.0       1.7
          30.0       1.9
          38.0       2.7
          39.0       8.7
          50.0       7.5
          51.0      14.2
          52.0       3.6
          62.0       2.0
          63.0       8.6
          64.0       4.9
          65.0       9.3
          66.0       1.2
          69.5       1.5
          70.5       1.5
          74.0       2.2
          75.0       2.6
          76.0       3.6
          77.0      16.9
          78.0       2.7
          83.5       5.5
          84.0       1.4
          89.0       3.0
          90.0       3.8
          91.0       2.1
         102.0       1.0
         103.0       1.6
         113.0       1.0
         114.0       1.4
         115.0       6.6
         116.0       1.6
         117.0       1.8
         127.0       1.5
         128.0       5.1
         129.0       4.6
         130.0       1.6
         139.0       7.4
         140.0       6.0
         141.0       3.8
         154.0       2.1
         155.0       1.1
         156.0       1.6
         166.0      13.3
         167.0      79.2
         168.0      36.1
         169.0       4.2
         184.0      31.6
         185.0       4.2
         198.0       1.3
         214.0     100.0
         215.0      13.9
         216.0       1.3
    

90 MHz in CDCl3

90 MHz in DMSO-d6


  • 1H NMR 89.56 MHz
    C12 H10 N2 O2 0.045 g : 0.5 ml CDCl3
    4-nitrodiphenylamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.082 B 7.50 to 7.03 C 6.933 D 6.50

         Hz     ppm     Int.
    

        732.19   8.176     74
        728.94   8.140    781
        726.88   8.117    227
        721.88   8.061    228
        719.75   8.037    966
        716.50   8.001    102
        670.19   7.484     83
        668.81   7.468    132
        667.00   7.448     99
        663.00   7.403    152
        661.63   7.388    274
        659.50   7.364    361
        657.44   7.341    128
        654.63   7.310    605
        653.94   7.302    540
        650.25   7.261    220
        647.88   7.235    917
        646.44   7.218    498
        644.88   7.201    169
        642.75   7.177    246
        640.94   7.157    332
        638.81   7.133    393
        635.31   7.094     77
        633.88   7.078     64
        632.06   7.058     89
        628.19   7.015    108
        625.13   6.981   1000
        623.00   6.957    263
        618.00   6.901    215
        615.88   6.877    826
        612.63   6.841     85
        582.44   6.504    138
    


  • 1H NMR 89.56 MHz
    C12 H10 N2 O2 0.036 g : 0.5 ml DMSO-d6
    4-nitrodiphenylamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.28 B 8.091 C 7.37 D 7.26 E 7.09 F 7.08 D AND E WERE CONFIRMED BY LAOCN PROGRAM.

         Hz     ppm     Int.
    

        831.44   9.284    248
        732.94   8.184     65
        729.69   8.148    780
        727.56   8.124    200
        722.56   8.068    210
        720.38   8.044    915
        717.13   8.008     95
        671.94   7.503     69
        670.81   7.491    140
        669.00   7.470     61
        664.94   7.425    179
        663.25   7.406    301
        662.06   7.393    296
        659.13   7.360     97
        656.56   7.331    592
        655.75   7.322    513
        654.75   7.311    390
        654.06   7.304    437
        652.38   7.285    762
        651.88   7.279    765
        649.06   7.248     95
        646.94   7.224    159
        645.25   7.205    256
        643.81   7.189    243
        642.38   7.173    187
        641.50   7.163    165
        640.19   7.149    100
        637.88   7.123   1000
        635.56   7.097    465
        632.50   7.063     78
        630.75   7.043    232
        628.50   7.018    749
        627.06   7.002     95
        626.13   6.992     47
        625.19   6.981     74
    

in CDCl3



KBr disc



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