-
MassMS-IW-2134 4,4'-(2,2,2-trifluoro-1-(trifluoromethyl)ethylidene)bis(2-aminophenol) C15H12F6N2O2 (Mass of molecular ion: 366)
Source Temperature: 170 °C Sample Temperature: 170 °C Direct, 75 eV
18.0 4.4 28.0 1.7 51.0 1.6 52.0 1.3 53.0 1.5 63.0 1.2 77.0 2.0 80.0 1.1 91.0 1.5 91.5 5.9 92.0 1.1 99.0 1.9 99.5 1.3 100.0 1.2 100.5 1.0 101.5 1.1 105.0 1.2 105.5 1.3 109.0 1.1 113.5 1.7 114.0 2.4 115.0 1.0 116.0 1.3 125.5 1.0 126.0 1.3 134.0 1.2 139.5 1.1 140.0 2.5 148.0 1.0 148.5 1.6 154.0 3.0 155.0 1.1 174.0 2.3 182.0 2.2 183.0 7.6 184.0 1.2 198.0 1.3 199.0 1.2 207.0 5.3 208.0 1.2 210.0 2.0 211.0 2.9 212.0 1.3 222.0 1.8 227.0 2.7 228.0 1.2 229.0 1.4 232.0 1.4 235.0 1.3 250.0 1.1 251.0 8.0 252.0 22.7 253.0 3.4 263.0 17.2 264.0 3.4 278.0 1.6 279.0 6.3 280.0 11.0 281.0 2.5 296.0 1.4 297.0 31.1 298.0 5.1 320.0 9.4 321.0 1.7 347.0 2.5 348.0 2.6 349.0 1.7 365.0 3.1 366.0 100.0 367.0 17.6 368.0 1.9
400 MHz in DMSO-d6
-
1H NMR 399.65 MHz C15 H12 F6 N2 O2 0.054 g : 0.5 ml DMSO-d6 4,4'-(2,2,2-trifluoro-1-(trifluoromethyl)ethylidene)bis(2-aminophenol) 
Assign. Shift(ppm)
A 9.4 B 6.669 C 6.595 D 6.445 E 4.7
Hz ppm Int.3767.09 9.426 65 2669.83 6.681 822 2661.44 6.660 1000 2650.15 6.632 23 2647.40 6.625 21 2635.04 6.594 675 2579.65 6.455 375 2571.41 6.435 318 1864.93 4.667 201
in DMSO-d6
KBr disc
nujol mull
更多供应商
