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MassMS-NW-5532 glycerol C3H8O3 (Mass of molecular ion: 92)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
14.0 1.5 15.0 27.4 17.0 1.6 18.0 6.9 19.0 5.0 26.0 2.1 27.0 6.2 28.0 5.9 29.0 15.2 30.0 3.8 31.0 29.0 32.0 1.8 33.0 1.8 42.0 5.4 43.0 74.1 44.0 46.3 45.0 4.6 55.0 2.0 56.0 2.3 57.0 1.2 60.0 9.1 61.0 100.0 62.0 5.0 74.0 1.2
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C3 H8 O3 0.05 ml : 0.5 ml DMSO-d6 glycerol 
Assign. Shift(ppm)
A 4.48 B 3.448 C *1 3.382 D *1 3.310
Hz ppm Int.1792.36 4.485 411 1390.63 3.480 72 1384.89 3.466 238 1379.64 3.453 453 1374.39 3.439 346 1368.90 3.426 203 1360.72 3.405 624 1355.59 3.392 316 1349.85 3.378 1000 1344.73 3.365 712 1334.72 3.340 34 1329.35 3.327 993 1323.49 3.312 744 1318.48 3.300 574 1312.62 3.285 435
in DMSO-d6
CCl4 solution
liquid film
4880 A,200 M,liquid
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