(S)-(-)-1-甲基-2-(1-萘胺甲基)吡咯烷

产品名称 (S)-(-)-1-甲基-2-(1-萘胺甲基)吡咯烷

CAS号82160-07-4

分子式C16H20N2

分子量240.34

¹³CNMR

Mass

MS-IW-4912          
(S)-N-(1-methyl-2-pyrrolidinylmethyl)-1-naphthylamine
C16H20N2            (Mass of molecular ion:    240)

   Source Temperature: 150 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      18.0       2.1
      42.0       5.5
      82.0       3.0
      83.0       1.2
      84.0     100.0
      85.0       6.3
     115.0       1.6
     127.0       2.2
     128.0       1.4
     143.0       1.1
     154.0       1.6
     155.0       1.0
     240.0       6.8
     241.0       1.3

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₆ H₂₀ N₂	0.039 g : 0.5 ml CDCl₃
(S)-N-(1-methyl-2-pyrrolidinylmethyl)-1-naphthylamine

    Assign.     Shift(ppm)

      A             7.838
      B             7.768
      C             7.43
      D             7.41
      E             7.335
      F             7.198
      G             6.564
      J             5.08
      K     *1      3.30
      L     *1      3.240
      M     *2      3.159
      N             2.571
      P             2.336
      Q     *2      2.274
      R     *3      1.95
      S     *4      1.90
      T     *3      1.83
      U     *4      1.75

     Hz     ppm     Int.

   3137.70   7.852     67
   3137.08   7.850     63
   3134.03   7.842     38
   3133.18   7.840     40
   3131.10   7.835     59
   3130.13   7.833     53
   3128.17   7.828     72
   3109.25   7.780     73
   3106.93   7.775     59
   3105.96   7.772     58
   3104.13   7.768     48
   3101.20   7.760     63
   3099.85   7.757     85
   2976.07   7.447     33
   2971.19   7.435    111
   2969.24   7.430    175
   2965.45   7.421    195
   2961.55   7.411    158
   2959.47   7.406     96
   2954.71   7.394     32
   2940.06   7.357     75
   2932.13   7.337    140
   2924.44   7.318    105
   2880.25   7.207    133
   2872.19   7.187     96
   2627.08   6.574    111
   2619.63   6.555    107
   2029.54   5.079     32
   1315.67   3.293     44
   1314.09   3.289     42
   1312.26   3.284     47
   1300.90   3.256     67
   1296.39   3.244     70
   1284.67   3.215     30
   1271.12   3.181     37
   1269.78   3.178     35
   1269.53   3.177     35
   1262.33   3.159     68
   1255.00   3.141     48
   1032.10   2.583     43
   1028.44   2.574     44
   1026.98   2.570     40
   1024.41   2.564     47
    933.84   2.337   1000
    922.24   2.308     50
    914.67   2.289     53
    912.60   2.284     76
    905.27   2.266     73
    903.44   2.261     59
    896.00   2.242     34
    787.11   1.970     42
    785.40   1.966     44
    778.93   1.950     50
    776.86   1.944     47
    771.85   1.932     36
    768.68   1.924     30
    766.11   1.917     48
    764.16   1.913     42
    762.21   1.908     45
    759.28   1.900     39
    754.64   1.889     55
    750.85   1.879     40
    749.27   1.875     34
    747.07   1.870     58
    742.19   1.858     35
    740.36   1.853     46
    737.67   1.846     34
    730.59   1.829     54
    704.35   1.763     40
    702.64   1.759     47
    700.68   1.754     45
    693.12   1.735     37
    691.28   1.730     30

in CDCl3

KBr disc

nujol mull

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(S)-(-)-1-甲基-2-(1-萘胺甲基)吡咯烷(82160-07-4)核磁图(¹³CNMR) 相关产品图谱

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