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MS-NW-3530 N-methylpyrrolidine C5H11N (Mass of molecular ion: 85)
Source Temperature: 290 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 12.8 18.0 3.3 26.0 2.1 27.0 8.6 28.0 8.0 29.0 3.6 30.0 4.2 38.0 1.0 39.0 6.7 40.0 1.9 41.0 10.7 42.0 100.0 43.0 9.4 44.0 3.7 53.0 1.1 54.0 2.4 55.0 6.6 56.0 3.3 57.0 89.7 58.0 4.2 67.0 1.9 68.0 1.5 69.0 1.0 70.0 1.5 82.0 9.4 83.0 2.0 84.0 97.2 85.0 55.8 86.0 3.4
90 MHz in CDCl3
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1H NMR 89.56 MHz C5 H11 N 0.04 ml : 0.5 ml CDCl3 N-methylpyrrolidine Assign. Shift(ppm)
A 2.47 B 2.353 C 1.78
Hz ppm Int.
228.06 2.547 35 224.81 2.511 67 223.56 2.497 67 220.88 2.467 142 218.88 2.444 105 217.19 2.426 65 217.00 2.423 65 215.50 2.407 69 214.31 2.393 77 210.81 2.354 1000 208.38 2.327 38 166.19 1.856 88 163.19 1.823 98 162.13 1.811 79 159.50 1.781 233 157.63 1.761 68 155.88 1.741 113 154.50 1.726 43 152.81 1.707 63
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