1,9-二氯壬烷

Mass

MS-NW-5661          
1,9-dichlorononane
C9H18Cl2            (Mass of molecular ion:    196)

   Source Temperature: 280 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      26.0       1.2
      27.0      22.9
      28.0       2.4
      29.0      21.6
      36.0       1.6
      39.0      16.8
      40.0       2.6
      41.0      71.6
      42.0      14.8
      43.0      34.2
      44.0       1.5
      49.0       5.1
      51.0       1.8
      53.0       5.8
      54.0       7.0
      55.0      93.3
      56.0      16.8
      57.0      11.9
      63.0       6.6
      65.0       2.5
      67.0       8.3
      68.0       9.7
      69.0      53.2
      70.0      11.6
      71.0       1.7
      75.0       1.3
      76.0       1.0
      77.0       3.9
      79.0       1.3
      81.0       5.5
      82.0      10.9
      83.0      22.6
      84.0       3.9
      90.0       2.2
      91.0     100.0
      92.0       6.0
      93.0      34.5
      94.0       1.9
      95.0       4.5
      96.0       2.3
      97.0       4.9
      98.0       1.3
     104.0      11.8
     105.0      11.9
     106.0       4.5
     107.0       3.9
     111.0       1.0
     118.0       5.9
     119.0       1.2
     120.0       2.0
     132.0       2.9

Assign. Shift(ppm) A 3.519 B 1.77 C 1.5 D 1.44 to 1.20 J(A,B)=6.6HZ.

     Hz     ppm     Int.

    322.38   3.600    369
    318.50   3.557     35
    315.94   3.528    968
    309.31   3.454    589
    164.81   1.841     93
    164.38   1.836     92
    162.69   1.817     84
    162.38   1.814     84
    161.88   1.808     85
    158.50   1.770    166
    158.19   1.767    167
    152.25   1.700    138
    151.25   1.689    128
    147.38   1.646     60
    147.06   1.643     60
    146.63   1.638     62
    146.38   1.635     62
    145.56   1.626     66
    145.00   1.620     67
    141.94   1.585     44
    141.63   1.582     46
    140.88   1.574     47
    140.44   1.569     49
    139.81   1.562     49
    139.44   1.557     49
    136.81   1.528     86
    133.94   1.496    119
    133.38   1.490    118
    132.50   1.480    113
    130.25   1.455    122
    118.44   1.323   1000
    109.50   1.223     31