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网站主页CAS数据库列表 4605-91-8更多图谱2 -甲基-双(六氯环戊二烯)(4605-91-8)核磁图(1HNMR)

2 -甲基-双(六氯环戊二烯)

产品名称 2 -甲基-双(六氯环戊二烯)

CAS号4605-91-8

分子式C21H10Cl12

分子量687.74

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  • Mass

    MS-NW-8519          
    2-methylnaphthalene-bis(hexachlorocyclopentadiene) adduct
    C21H10Cl12          (Mass of molecular ion:    682)
    

       Source Temperature: 220 °C
       Sample Temperature: 140 °C
       Direct, 75 eV
    

         115.0       2.4
         141.0      10.3
         142.0     100.0
         143.0      12.0
         237.0       1.0
         414.0       1.4
         416.0       1.1
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C21 H10 Cl12 0.046 g : 0.5 ml CDCl3
    2-methylnaphthalene-bis(hexachlorocyclopentadiene) adduct
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.57 B 7.51 C 7.08 D 3.93 E 3.52 F 2.343

         Hz     ppm     Int.
    

        683.31   7.630    157
        674.94   7.537    260
        673.50   7.521    217
        672.94   7.514    226
        672.56   7.510    221
        672.19   7.506    225
        638.56   7.130    118
        638.19   7.126    117
        637.75   7.121    115
        636.88   7.112    119
        630.69   7.043     90
        630.25   7.038     89
        629.38   7.028     84
        629.06   7.024     89
        357.88   3.996    172
        357.44   3.992    166
        348.50   3.892    281
        319.56   3.569    249
        318.50   3.557    586
        309.63   3.458    357
        308.50   3.445    157
        209.94   2.345   1000
    

KBr disc



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