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MS-NW-3794 1,2-propanedithiol C3H8S2 (Mass of molecular ion: 108)
Source Temperature: 270 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 1.6 18.0 1.1 26.0 1.8 27.0 13.1 29.0 1.4 32.0 3.3 33.0 4.2 34.0 7.3 35.0 12.4 37.0 2.0 38.0 2.7 39.0 22.7 40.0 3.4 41.0 80.4 42.0 7.5 43.0 1.6 44.0 2.0 45.0 24.1 46.0 8.6 47.0 39.4 48.0 2.0 49.0 2.4 57.0 1.8 58.0 5.8 59.0 20.5 60.0 26.5 61.0 100.0 62.0 4.2 63.0 4.8 64.0 1.0 69.0 1.4 71.0 2.0 73.0 4.6 74.0 50.6 75.0 21.5 76.0 3.3 77.0 2.0 108.0 45.7 109.0 2.5 110.0 4.4 121.0 1.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C3 H8 S2 0.04 ml : 0.5 ml CDCl3 1,2-propanedithiol Assign. Shift(ppm)
A 3.02 B *1 2.73 C *1 2.69 D 1.832 E 1.641 F 1.400
Hz ppm Int.
286.44 3.199 47 280.56 3.133 73 279.63 3.123 100 274.00 3.060 119 273.06 3.049 100 267.13 2.983 136 266.13 2.972 65 260.69 2.911 96 254.81 2.846 36 250.19 2.794 578 244.69 2.733 194 243.25 2.717 143 242.06 2.703 429 241.38 2.696 360 235.63 2.631 375 167.56 1.871 317 167.06 1.866 284 161.00 1.798 296 160.50 1.793 260 154.56 1.726 407 146.56 1.637 325 145.69 1.627 255 137.69 1.538 272 128.81 1.439 1000 122.25 1.366 986 119.44 1.334 36
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