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MassMS-IW-2217 2-(trimethylsilyl)thiazole C6H11NSSi (Mass of molecular ion: 157)
Source Temperature: 220 °C Sample Temperature: 160 °C Reservoir, 75 eV
29.0 2.2 42.0 1.3 43.0 9.6 44.0 2.7 45.0 9.5 53.0 1.2 54.0 1.9 55.0 1.4 56.0 2.5 57.0 4.4 58.0 16.1 59.0 3.9 60.0 1.1 68.0 1.3 70.0 2.3 71.0 1.0 72.0 3.8 73.0 29.4 74.0 2.6 75.0 4.8 84.0 18.8 85.0 8.1 86.0 2.2 90.0 1.8 91.0 1.3 98.0 6.7 99.0 1.2 101.0 1.3 112.0 1.0 115.0 6.4 116.0 8.2 117.0 1.4 142.0 100.0 143.0 11.9 144.0 8.5 147.0 7.8 148.0 1.2 155.0 5.4 156.0 1.4 157.0 41.5 158.0 5.4 159.0 3.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H11 N S Si 0.05 ml : 0.5 ml CDCl3 2-(trimethylsilyl)thiazole 
Assign. Shift(ppm)
A 8.117 B 7.511 C 0.414 J(A,B)=3.1HZ J(C,SI-29)=7.0HZ
Hz ppm Int.3245.73 8.122 111 3242.68 8.114 113 3003.30 7.515 155 3000.24 7.508 151 169.07 0.424 189 165.77 0.415 1000 162.11 0.406 149
in CDCl3
liquid film
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