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网站主页CAS数据库列表 79265-30-8更多图谱2-(三甲基硅基)噻唑(79265-30-8)核磁图(13CNMR)

2-(三甲基硅基)噻唑

产品名称 2-(三甲基硅基)噻唑

CAS号79265-30-8

分子式C6H11NSSi

分子量157.31

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  • Mass

    MS-IW-2217          
    2-(trimethylsilyl)thiazole
    C6H11NSSi           (Mass of molecular ion:    157)
    

       Source Temperature: 220 °C
       Sample Temperature: 160 °C
       Reservoir, 75 eV
    

          29.0       2.2
          42.0       1.3
          43.0       9.6
          44.0       2.7
          45.0       9.5
          53.0       1.2
          54.0       1.9
          55.0       1.4
          56.0       2.5
          57.0       4.4
          58.0      16.1
          59.0       3.9
          60.0       1.1
          68.0       1.3
          70.0       2.3
          71.0       1.0
          72.0       3.8
          73.0      29.4
          74.0       2.6
          75.0       4.8
          84.0      18.8
          85.0       8.1
          86.0       2.2
          90.0       1.8
          91.0       1.3
          98.0       6.7
          99.0       1.2
         101.0       1.3
         112.0       1.0
         115.0       6.4
         116.0       8.2
         117.0       1.4
         142.0     100.0
         143.0      11.9
         144.0       8.5
         147.0       7.8
         148.0       1.2
         155.0       5.4
         156.0       1.4
         157.0      41.5
         158.0       5.4
         159.0       3.5
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C6 H11 N S Si 0.05 ml : 0.5 ml CDCl3
    2-(trimethylsilyl)thiazole
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.117 B 7.511 C 0.414 J(A,B)=3.1HZ J(C,SI-29)=7.0HZ

         Hz     ppm     Int.
    

       3245.73   8.122    111
       3242.68   8.114    113
       3003.30   7.515    155
       3000.24   7.508    151
        169.07   0.424    189
        165.77   0.415   1000
        162.11   0.406    149
    

in CDCl3



liquid film