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1-乙基金刚烷

产品名称 1-乙基金刚烷

CAS号770-69-4

分子式C12H20

分子量164.29

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  • Mass

    MS-IW-4051          
    1-ethyladamantane
    C12H20              (Mass of molecular ion:    164)
    

       Source Temperature: 240 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          29.0       1.4
          39.0       1.2
          41.0       4.1
          53.0       1.3
          55.0       3.1
          67.0       6.1
          69.0       1.6
          77.0       2.8
          79.0      16.2
          80.0       1.4
          81.0       4.1
          91.0       3.0
          93.0      13.3
          94.0       1.3
         107.0       7.1
         135.0     100.0
         136.0      11.1
         164.0       3.8
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C12 H20 0.05 ml : 0.5 ml CDCl3
    1-ethyladamantane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 1.936 B *1 1.695 C *1 1.624 D 1.441 E 1.079 F 0.775

         Hz     ppm     Int.
    

        773.80   1.937    311
        685.42   1.716    149
        673.58   1.686    299
        657.35   1.645    114
        656.13   1.642    201
        653.56   1.636    306
        652.59   1.633    292
        649.54   1.626    176
        648.44   1.623    120
        644.90   1.614     74
        643.92   1.612    101
        641.36   1.605    155
        639.89   1.602    148
        637.21   1.595     91
        577.15   1.445    934
        574.46   1.438    878
        443.60   1.110    107
        435.91   1.091    359
        428.34   1.072    396
        420.90   1.054    158
        316.77   0.793    560
        309.45   0.775   1000
        301.64   0.755    430
    

in CDCl3



liquid film