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MS-IW-4051 1-ethyladamantane C12H20 (Mass of molecular ion: 164)
Source Temperature: 240 °C Sample Temperature: 150 °C Reservoir, 75 eV
29.0 1.4 39.0 1.2 41.0 4.1 53.0 1.3 55.0 3.1 67.0 6.1 69.0 1.6 77.0 2.8 79.0 16.2 80.0 1.4 81.0 4.1 91.0 3.0 93.0 13.3 94.0 1.3 107.0 7.1 135.0 100.0 136.0 11.1 164.0 3.8
400 MHz in CDCl3
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1H NMR 399.65 MHz C12 H20 0.05 ml : 0.5 ml CDCl3 1-ethyladamantane Assign. Shift(ppm)
A 1.936 B *1 1.695 C *1 1.624 D 1.441 E 1.079 F 0.775
Hz ppm Int.
773.80 1.937 311 685.42 1.716 149 673.58 1.686 299 657.35 1.645 114 656.13 1.642 201 653.56 1.636 306 652.59 1.633 292 649.54 1.626 176 648.44 1.623 120 644.90 1.614 74 643.92 1.612 101 641.36 1.605 155 639.89 1.602 148 637.21 1.595 91 577.15 1.445 934 574.46 1.438 878 443.60 1.110 107 435.91 1.091 359 428.34 1.072 396 420.90 1.054 158 316.77 0.793 560 309.45 0.775 1000 301.64 0.755 430
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