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网站主页CAS数据库列表 77-06-5更多图谱赤霉素(77-06-5)核磁图(13CNMR)

赤霉素

产品名称 赤霉素

CAS号77-06-5

分子式C19H22O6

分子量346.38

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  • Mass

    MS-NW-8567          
    gibberellic acid
    C19H22O6            (Mass of molecular ion:    346)
    

       Source Temperature: 220 °C
       Sample Temperature: 200 °C
       Direct, 75 eV
    

          17.0       2.1
          18.0      10.8
          27.0      11.8
          28.0       7.5
          29.0      12.9
          31.0       3.4
          36.0       1.2
          39.0      18.5
          40.0       7.3
          41.0      32.2
          42.0       3.1
          43.0      40.8
          44.0      13.2
          45.0       3.9
          50.0       1.7
          51.0       8.8
          52.0       3.6
          53.0      16.1
          54.0       2.5
          55.0      36.7
          56.0       3.5
          57.0       8.0
          58.0       1.0
          63.0       4.2
          64.0       2.4
          65.0      14.5
          66.0       4.8
          67.0      11.8
          68.0       4.8
          69.0      15.5
          70.0       2.6
          71.0       4.7
          73.0       1.3
          75.0       1.9
          76.0       2.7
          77.0      32.3
          78.0       9.6
          79.0      23.5
          80.0       4.4
          81.0      10.9
          82.0       4.1
          82.5       1.0
          83.0       8.5
          84.0       5.9
          85.0       6.2
          86.0       1.4
          87.0       1.4
          89.0       5.3
          90.0       2.9
          91.0      39.2
          92.0       7.3
          93.0      11.6
          94.0       5.4
          95.0      22.8
          96.0       5.8
          97.0       6.0
          98.0       5.0
          99.0       4.8
         100.0       1.4
         101.0       2.1
         102.0       2.9
         103.0       8.6
         104.0       4.8
         105.0      21.6
         106.0       5.7
         107.0      18.5
         108.0      14.2
         109.0      18.8
         110.0       3.1
         111.0       8.7
         112.0       3.7
         113.0       2.5
         114.0       2.1
         115.0      23.8
         116.0       8.1
         117.0      13.2
         118.0       5.1
         119.0      12.1
         120.0       5.3
         121.0      54.2
         122.0      19.3
         123.0       6.5
         124.0       3.7
         125.0       1.9
         126.0       1.7
         127.0      12.3
         128.0      21.5
         129.0      19.4
         130.0       6.0
         131.0      14.3
         132.0       6.2
         133.0      13.5
         134.0      19.7
         135.0      31.1
         136.0     100.0
         137.0      24.9
         138.0       3.0
         139.0       3.7
         140.0       1.7
         141.0      17.1
         142.0      12.3
         143.0      14.7
         144.0       8.7
         145.0      16.8
         146.0       5.8
         147.0      11.5
         148.0       6.5
         149.0      14.2
         150.0       7.5
         151.0      11.7
         152.0      28.6
         153.0      23.4
         154.0       7.7
         155.0      22.9
         156.0      14.4
         157.0      16.8
         158.0       7.9
         159.0      13.1
         160.0       5.4
         161.0       9.8
         162.0       3.5
         163.0      10.7
         164.0       4.6
         165.0      15.8
         166.0       8.4
         167.0       9.3
         168.0       5.6
         169.0      15.4
         170.0       6.2
         171.0      13.8
         172.0      10.0
         173.0      14.5
         174.0       7.3
         175.0       8.5
         176.0       5.6
         177.0       5.5
         178.0       6.6
         179.0      12.5
         180.0       7.4
         181.0      15.7
         182.0       7.9
         183.0      12.3
         184.0       5.4
         185.0      15.6
         186.0       6.3
         187.0       8.4
         188.0       5.1
         189.0       9.2
         190.0       7.1
         191.0      10.7
         192.0       6.2
         193.0      11.0
         194.0       7.0
         195.0      21.4
         196.0       9.1
         197.0      14.8
         198.0       7.3
         199.0      13.0
         200.0      10.9
         201.0       9.6
         202.0      17.1
         203.0      23.2
         204.0       5.6
         205.0       4.5
         206.0       4.0
         207.0       6.1
         208.0       4.4
         209.0      28.3
         210.0      12.5
         211.0      15.8
         212.0       7.1
         213.0      13.5
         214.0       5.8
         215.0       7.8
         216.0       7.4
         217.0       5.9
         218.0       5.3
         219.0      15.2
         220.0       9.3
         221.0      11.9
         222.0       5.2
         223.0      15.6
         224.0       7.2
         225.0      16.8
         226.0      10.9
         227.0      16.6
         228.0       8.0
         229.0       6.8
         230.0       4.4
         231.0       6.3
         232.0       3.0
         233.0       2.2
         234.0       1.1
         235.0       1.7
         236.0       3.7
         237.0      27.9
         238.0      21.6
         239.0      25.4
         240.0      11.4
         241.0      14.0
         242.0       8.2
         243.0      10.3
         244.0      11.9
         245.0       8.9
         246.0       2.4
         247.0       1.5
         248.0       1.2
         249.0       2.1
         251.0       3.6
         252.0       1.4
         253.0       6.7
         254.0      13.2
         255.0      26.4
         256.0      18.0
         257.0       9.0
         258.0       7.4
         259.0       4.0
         260.0       2.0
         261.0       2.5
         262.0       1.8
         264.0       3.8
         265.0       7.7
         266.0      11.8
         267.0       8.0
         268.0       4.1
         269.0       9.8
         270.0       3.0
         271.0       7.2
         272.0      10.8
         273.0       9.0
         274.0       3.9
         275.0       1.1
         281.0       2.8
         282.0      22.5
         283.0      29.4
         284.0      41.7
         285.0      14.6
         286.0       5.8
         287.0       6.0
         288.0       1.6
         289.0       2.5
         290.0       4.1
         291.0       1.1
         292.0       1.6
         295.0       2.5
         299.0       4.6
         300.0      43.5
         301.0      21.9
         302.0      15.0
         303.0       4.4
         304.0       1.3
         305.0       1.2
         310.0      14.8
         311.0       3.6
         312.0       1.7
         313.0       2.9
         317.0       6.0
         318.0       3.8
         319.0       1.0
         328.0      44.9
         329.0      10.0
         330.0      11.4
         331.0       4.5
         346.0      26.5
         347.0       5.7
         348.0       4.6
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C19 H22 O6 0.036 g : 0.5 ml DMSO-d6
    gibberellic acid
    ChemicalStructure
        Assign.     Shift(ppm)
    A 12.6 B 6.334 C 5.800 D 5.58 E *1 5.127 F 4.87 G *1 4.85 J 3.874 K 3.075 L 2.50 M *2 2.18 N *2 2.15 P *3 1.91 Q *3 1.86 R *4 1.72 S 1.77 to 1.460 T *4 1.63 U 1.071 J(B,C)=9.3HZ. J(C,J)=3.7HZ. J(D,J)=6.6HZ. J(K,L)=10.8HZ. ASSIGNED BY H-H COSY.

         Hz     ppm     Int.
    

       2536.49   6.347    122
       2536.12   6.346    124
       2526.78   6.323    139
       2324.20   5.816    100
       2320.54   5.807     96
       2314.86   5.793     89
       2311.19   5.784     93
       2234.45   5.592    102
       2227.85   5.575    102
       2049.08   5.128    114
       1944.13   4.865    196
       1939.92   4.855    139
       1552.89   3.886     59
       1549.41   3.877     66
       1546.66   3.871     66
       1543.18   3.862     57
       1234.73   3.090    154
       1223.92   3.063    168
       1011.99   2.533     32
       1005.58   2.517    329
       1003.75   2.512    676
       1001.92   2.507   1000
       1000.09   2.503    636
        998.26   2.498    289
        991.30   2.481    149
        867.66   2.172    105
        864.73   2.164     90
        861.98   2.157    101
        772.23   1.933     38
        764.90   1.914     54
        763.62   1.911     46
        762.89   1.909     47
        762.34   1.908     45
        758.49   1.898     41
        755.74   1.892     31
        755.20   1.890     32
        754.83   1.889     33
        754.28   1.888     33
        752.81   1.884     36
        751.90   1.882     38
        751.53   1.881     38
        750.80   1.879     37
        749.70   1.876     33
        749.15   1.875     32
        748.24   1.873     33
        747.50   1.871     35
        747.14   1.870     35
        744.39   1.863     68
        742.37   1.858     41
        740.73   1.854     48
        740.36   1.853     47
        733.95   1.837     54
        695.12   1.740     52
        694.57   1.738     52
        693.65   1.736     52
        684.13   1.712     97
        674.24   1.688     35
        673.69   1.686     33
        668.74   1.674     37
        663.43   1.661    173
        659.58   1.651     58
        652.81   1.634    149
        648.78   1.624    168
        642.18   1.607     54
        641.82   1.606     55
        641.45   1.606     55
        637.97   1.597     32
        637.60   1.596     33
        637.24   1.595     33
        433.74   1.086     50
        428.06   1.072    767
    

in DMSO-d6



KBr disc