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MassMS-IW-9299 tert-butyl 2,3-epoxypropyl ether C7H14O2 (Mass of molecular ion: 130)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 2.4 27.0 7.7 28.0 2.7 29.0 44.0 30.0 1.2 31.0 16.3 39.0 4.5 41.0 22.7 42.0 1.9 43.0 6.2 44.0 1.4 45.0 1.2 55.0 2.4 56.0 7.7 57.0 100.0 58.0 4.4 59.0 23.3 73.0 1.7 115.0 36.2 116.0 2.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H14 O2 0.05 ml : 0.5 ml CDCl3 tert-butyl 2,3-epoxypropyl ether 
Assign. Shift(ppm)
A *1 3.549 B *1 3.397 C 3.099 D 2.793 E 2.614 F 1.209
Hz ppm Int.1426.64 3.570 66 1422.85 3.561 68 1415.89 3.543 91 1412.11 3.534 93 1365.11 3.416 79 1359.74 3.403 85 1354.37 3.389 57 1349.00 3.376 63 1243.77 3.113 32 1242.68 3.110 49 1240.97 3.106 35 1239.99 3.103 52 1238.65 3.100 53 1237.18 3.096 49 1235.96 3.093 37 1234.50 3.089 46 1233.28 3.086 32 1120.73 2.805 83 1116.70 2.795 86 1115.60 2.792 107 1111.57 2.782 88 1047.97 2.623 90 1045.29 2.616 89 1042.85 2.610 81 1040.16 2.603 78 483.40 1.210 1000
in CDCl3
liquid film
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