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MassMS-IW-0561 N,N-dibutylformamide C9H19NO (Mass of molecular ion: 157)
Source Temperature: 270 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 3.9 28.0 4.1 29.0 13.5 30.0 18.2 39.0 2.7 41.0 12.1 42.0 3.9 43.0 2.0 44.0 12.0 46.0 2.6 55.0 3.6 56.0 2.2 57.0 9.7 58.0 14.0 59.0 4.5 60.0 2.0 72.0 100.0 73.0 13.7 84.0 2.0 85.0 1.5 86.0 3.5 98.0 1.6 100.0 4.6 102.0 2.2 114.0 69.1 115.0 6.8 128.0 5.6 142.0 1.5 157.0 1.9 158.0 4.6
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H19 N O 0.05 ml : 0.5 ml CDCl3 N,N-dibutylformamide 
Assign. Shift(ppm)
A 8.051 B 3.296 C 3.216 D 1.53 E 1.52 F 1.325 G 1.316 J 0.942 K 0.933
Hz ppm Int.3217.53 8.051 480 1325.07 3.316 277 1317.50 3.297 311 1315.55 3.292 131 1309.81 3.278 295 1292.85 3.235 266 1285.64 3.217 432 1278.44 3.199 288 627.44 1.570 64 620.12 1.552 154 616.33 1.543 110 614.26 1.537 190 612.67 1.534 292 609.99 1.527 160 607.06 1.519 282 605.59 1.516 216 604.49 1.513 223 601.07 1.504 127 599.61 1.501 167 597.78 1.496 184 592.04 1.482 93 548.58 1.373 49 543.95 1.362 60 541.26 1.355 149 536.50 1.343 172 533.81 1.336 213 528.93 1.324 232 526.00 1.317 221 521.24 1.305 225 518.68 1.298 161 514.04 1.287 144 511.35 1.280 60 506.71 1.268 48 383.79 0.961 492 380.37 0.952 517 376.34 0.942 923 372.92 0.934 1000 369.02 0.924 482 365.60 0.915 493
in CDCl3
liquid film
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