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网站主页CAS数据库列表 4559-86-8更多图谱四丁基脲(4559-86-8)核磁图(13CNMR)

四丁基脲

产品名称 四丁基脲

CAS号4559-86-8

分子式C17H36N2O

分子量284.48

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  • Mass

    MS2014-05046CW      
    tetrabutylurea
    C17H36N2O           (Mass of molecular ion:    284)
    

       Source Temperature: 250 °C
       Sample Temperature: 250 °C
       Reservoir, 70 eV
    

          27.0       1.9
          28.0      16.4
          29.0      10.2
          30.0       2.7
          32.0       4.0
          39.0       1.2
          41.0      14.4
          42.0       3.7
          43.0       2.8
          44.0       3.3
          55.0       3.5
          56.0       2.8
          57.0      57.4
          58.0       2.7
          70.0       1.3
          72.0       1.4
          84.0       4.0
          86.0      22.2
          87.0       1.3
          99.0       1.3
         100.0      16.6
         101.0       1.1
         112.0       1.0
         114.0       1.0
         128.0      34.0
         129.0       4.6
         130.0       1.4
         155.0       2.7
         156.0     100.0
         157.0      10.0
         185.0       2.9
         227.0       1.5
         228.0       1.6
         241.0       8.4
         242.0       1.4
         284.0       6.6
         285.0       1.3
    

400 MHz in CDCl3

in CDCl3


  • 1H NMR 399.65 MHz
    C17 H36 N2 O 0.04 ml : 0.5 ml CDCl3
    tetrabutylurea
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.102 B 1.479 C 1.283 D 0.912

         Hz     ppm     Int.
    

       1246.95   3.121    273
       1239.50   3.102    290
       1237.55   3.097    136
       1232.06   3.083    266
        606.57   1.518     61
        599.37   1.500    127
        597.05   1.494     95
        593.75   1.486    113
        591.55   1.481    210
        588.75   1.474    104
        585.45   1.465    116
        584.11   1.462    136
        582.15   1.457     95
        576.54   1.443     73
        530.52   1.328     52
        523.07   1.309    147
        515.63   1.291    198
        507.93   1.271    190
        500.61   1.253    122
        493.41   1.235     39
        377.08   0.944     33
        371.58   0.930    545
        364.26   0.912   1000
        356.93   0.894    422
    



in CDCl3



liquid film