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MS-NW-8201 tetrabutylammonium chloride C16H36ClN (Mass of molecular ion: 277)
Source Temperature: 180 °C Sample Temperature: 190 °C Direct, 75 eV
26.0 1.1 27.0 8.9 28.0 20.7 29.0 17.6 30.0 6.8 39.0 4.6 41.0 24.5 42.0 7.9 43.0 8.2 44.0 11.4 55.0 4.9 56.0 19.0 57.0 15.5 58.0 8.9 70.0 1.7 72.0 1.2 84.0 3.2 86.0 3.5 98.0 3.7 100.0 46.4 101.0 3.4 128.0 1.1 142.0 100.0 143.0 10.6 184.0 1.2 185.0 6.5 186.0 1.1 242.0 2.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C16 H36 Cl N 0.046 g : 0.5 ml CDCl3 tetrabutylammonium chloride Assign. Shift(ppm)
A 3.40 B 1.67 C 1.45 D 1.02
Hz ppm Int.
328.63 3.670 33 328.13 3.664 32 306.06 3.418 274 302.06 3.373 250 301.19 3.363 250 300.75 3.359 250 300.31 3.354 250 299.56 3.345 249 297.56 3.323 255 140.56 1.570 376 135.13 1.509 308 127.75 1.427 264 121.06 1.352 173 109.75 1.226 37 109.31 1.221 36 108.56 1.213 36 107.56 1.201 34 106.94 1.195 33 106.25 1.187 33 106.13 1.186 33 96.25 1.075 581 90.31 1.009 1000 83.94 0.938 306
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