90 MHz in CDCl3
parameter in CDCl3
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1H NMR 89.56 MHz C2 H5 I 0.04 ml : 0.5 ml CDCl3 iodoethane Assign. Shift(ppm)
A 3.186 B 1.847 J(A,B)=7.6HZ
Hz ppm Int.
297.69 3.324 92 297.00 3.317 93 289.81 3.236 341 282.94 3.160 221 282.31 3.153 404 275.31 3.075 133 274.69 3.068 127 172.38 1.925 406 165.19 1.845 1000 164.75 1.840 593 157.50 1.759 311
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1H NMR 300 MHz C2 H5 I 10 vol% in CCl4 iodoethane Parameter ppm Hz
D(A) 1.859 D(B) 3.155 J(A,B) 7.446 EBERSOLE,S. ET AL. J.PHYS.CHEM. 68, 3430 (1964)
Hz ppm Int.
957.78 3.193 152 950.32 3.168 472 942.88 3.143 489 935.45 3.118 170 565.08 1.884 509 557.64 1.859 1000 550.19 1.834 467
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