4,9-二噁-1,12十二烷二胺

Mass

MS-IW-0973          
3,3'-(tetramethylenedioxy)dipropylamine
C10H24N2O2          (Mass of molecular ion:    204)

   Source Temperature: 230 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      17.0       3.2
      18.0      19.2
      27.0       3.1
      28.0       9.7
      29.0       5.2
      30.0     100.0
      31.0       6.7
      39.0       2.1
      41.0      16.0
      42.0       7.1
      43.0      10.3
      44.0      11.6
      45.0      12.9
      54.0       1.6
      55.0      10.3
      56.0      31.3
      57.0      50.8
      58.0      80.9
      59.0      22.7
      60.0       1.2
      69.0       1.1
      70.0       3.0
      71.0      16.1
      72.0       3.1
      73.0       6.2
      74.0      35.5
      75.0       9.1
      76.0      26.5
      77.0       1.3
      81.0       1.0
      84.0       2.0
      85.0       2.4
      86.0       3.4
      88.0       1.4
     100.0      11.6
     101.0       1.3
     103.0       1.7
     114.0      14.4
     115.0       1.3
     117.0       4.9
     130.0      10.1
     131.0       5.9
     146.0      29.3
     147.0       2.8
     148.0      41.8
     149.0       3.5
     205.0       1.2

Assign. Shift(ppm) A 3.482 B 3.42 C 2.778 D 1.70 E 1.62 F 1.22

     Hz     ppm     Int.

    327.81   3.661     30
    325.63   3.636     39
    324.69   3.626     42
    318.19   3.553    444
    311.94   3.484   1000
    308.81   3.449    313
    306.19   3.419    759
    301.25   3.364    180
    300.31   3.354    180
    298.06   3.329     46
    297.56   3.323     47
    256.13   2.860    312
    249.31   2.784    691
    245.94   2.747     69
    242.63   2.710    416
    164.69   1.839    126
    158.50   1.770    404
    152.06   1.698    590
    147.88   1.652    339
    145.25   1.622    756
    142.50   1.592    265
    139.06   1.553    213
    136.44   1.524     55
    108.88   1.216    985