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MassMS-IW-0973 3,3'-(tetramethylenedioxy)dipropylamine C10H24N2O2 (Mass of molecular ion: 204)
Source Temperature: 230 °C Sample Temperature: 150 °C Reservoir, 75 eV
17.0 3.2 18.0 19.2 27.0 3.1 28.0 9.7 29.0 5.2 30.0 100.0 31.0 6.7 39.0 2.1 41.0 16.0 42.0 7.1 43.0 10.3 44.0 11.6 45.0 12.9 54.0 1.6 55.0 10.3 56.0 31.3 57.0 50.8 58.0 80.9 59.0 22.7 60.0 1.2 69.0 1.1 70.0 3.0 71.0 16.1 72.0 3.1 73.0 6.2 74.0 35.5 75.0 9.1 76.0 26.5 77.0 1.3 81.0 1.0 84.0 2.0 85.0 2.4 86.0 3.4 88.0 1.4 100.0 11.6 101.0 1.3 103.0 1.7 114.0 14.4 115.0 1.3 117.0 4.9 130.0 10.1 131.0 5.9 146.0 29.3 147.0 2.8 148.0 41.8 149.0 3.5 205.0 1.2
90 MHz in CDCl3
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1H NMR 89.56 MHz C10 H24 N2 O2 0.05 ml : 0.5 ml CDCl3 3,3'-(tetramethylenedioxy)dipropylamine 
Assign. Shift(ppm)
A 3.482 B 3.42 C 2.778 D 1.70 E 1.62 F 1.22
Hz ppm Int.327.81 3.661 30 325.63 3.636 39 324.69 3.626 42 318.19 3.553 444 311.94 3.484 1000 308.81 3.449 313 306.19 3.419 759 301.25 3.364 180 300.31 3.354 180 298.06 3.329 46 297.56 3.323 47 256.13 2.860 312 249.31 2.784 691 245.94 2.747 69 242.63 2.710 416 164.69 1.839 126 158.50 1.770 404 152.06 1.698 590 147.88 1.652 339 145.25 1.622 756 142.50 1.592 265 139.06 1.553 213 136.44 1.524 55 108.88 1.216 985
in CDCl3
liquid film
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