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网站主页CAS数据库列表 7242-92-4更多图谱外-2-氨基降冰片烷(7242-92-4)核磁图(1HNMR)

外-2-氨基降冰片烷

产品名称 外-2-氨基降冰片烷

CAS号7242-92-4

分子式C7H13N

分子量111.18

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  • Mass

    MS-NW-5766          
    exo-2-aminonorbornane
    C7H13N              (Mass of molecular ion:    111)
    

       Source Temperature: 250 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          15.0       3.3
          18.0       9.6
          26.0       1.5
          27.0      12.3
          28.0      25.9
          29.0       5.5
          30.0      59.5
          31.0       1.3
          38.0       2.0
          39.0      19.0
          40.0       3.9
          41.0      20.6
          42.0      16.9
          43.0      70.9
          44.0      16.3
          45.0      29.9
          50.0       1.6
          51.0       3.0
          52.0       2.0
          53.0       6.4
          54.0       6.2
          55.0       5.0
          56.0      77.2
          57.0      23.6
          58.0       1.1
          65.0       5.5
          66.0      22.1
          67.0      22.5
          68.0       6.2
          69.0      16.0
          70.0      35.5
          71.0       2.2
          77.0       4.5
          78.0       1.7
          79.0      38.5
          80.0       5.9
          81.0       3.5
          82.0     100.0
          83.0      21.1
          84.0       1.9
          91.0       2.3
          93.0       4.8
          94.0      40.5
          95.0       4.9
          96.0       9.6
          97.0       1.0
         110.0      12.1
         111.0      57.6
         112.0       4.9
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C7 H13 N 0.05 ml : 0.5 ml CDCl3
    exo-2-aminonorbornane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.805 B 2.207 C 1.925 D 1.633 E 1.46 to 1.42 F 1.09 G 1.06 J 1.05 K 1.01 ASSIGNED BY C-H COSY

         Hz     ppm     Int.
    

       1126.59   2.819    323
       1123.29   2.811    333
       1119.02   2.800    345
       1115.72   2.792    339
        882.20   2.208    502
        771.12   1.930    521
        767.46   1.921    488
        664.43   1.663    277
        661.99   1.657    280
        656.74   1.644    276
        654.30   1.638    289
        651.73   1.631    320
        649.29   1.625    319
        644.04   1.612    310
        641.72   1.606    309
        591.43   1.480    432
        589.72   1.476    575
        587.77   1.471    539
        585.94   1.467    565
        583.50   1.461    411
        581.54   1.456    767
        579.71   1.451    910
        578.25   1.447   1000
        576.05   1.442    717
        574.34   1.438    923
        570.19   1.427    645
        566.77   1.419    483
        565.55   1.416    508
        562.74   1.409    417
        444.34   1.112    474
        442.99   1.109    540
        441.89   1.106    586
        440.67   1.103    474
        434.45   1.088    409
        433.11   1.084    586
        432.01   1.081    748
        430.66   1.078    590
        423.83   1.061    791
        421.88   1.056    739
        416.87   1.044    571
        414.79   1.038    572
        405.03   1.014    377
    

in CDCl3



liquid film