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MassMS-NW-0299 DL-lysine monohydrochloride C6H14N2O2 HCl (Mass of molecular ion: 146)
Source Temperature: 190 °C Sample Temperature: 0 °C Direct, 75 eV
15.0 2.2 16.0 2.1 17.0 3.8 18.0 14.4 26.0 2.4 27.0 9.9 28.0 29.7 29.0 8.1 30.0 100.0 31.0 2.2 35.0 7.5 36.0 60.4 37.0 2.5 38.0 19.9 39.0 9.1 40.0 2.6 41.0 19.3 42.0 18.5 43.0 34.0 44.0 13.9 45.0 3.3 46.0 2.0 50.0 1.2 51.0 1.9 52.0 2.7 53.0 3.5 54.0 14.0 55.0 25.1 56.0 71.7 57.0 13.4 58.0 3.4 59.0 4.2 65.0 1.4 66.0 1.8 67.0 7.5 68.0 3.9 69.0 4.7 70.0 10.3 71.0 8.6 72.0 57.7 73.0 4.5 74.0 12.5 75.0 3.3 79.0 1.7 80.0 2.9 81.0 3.2 82.0 19.3 83.0 33.1 84.0 76.0 85.0 6.0 87.0 1.4 88.0 1.5 89.0 2.1 93.0 2.5 99.0 4.2 100.0 5.4 101.0 3.9 109.0 2.5 110.0 6.0 111.0 7.2 112.0 1.1 117.0 1.8 128.0 4.0 129.0 7.1 130.0 3.0
90 MHz in D2O
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1H NMR 89.56 MHz C6 H14 N2 O2 0.044 g : 0.5 ml D2O DL-lysine monohydrochloride 
Assign. Shift(ppm)
B 3.764 C 3.032 D 1.95 to 1.34 THE SOLVENT SIGNAL REMOVED.
Hz ppm Int.343.38 3.835 351 337.69 3.771 812 331.69 3.704 487 279.56 3.122 545 272.81 3.047 1000 265.25 2.962 857 170.44 1.904 549 167.63 1.872 732 164.50 1.837 594 161.94 1.809 679 157.69 1.761 584 155.38 1.735 551 151.69 1.694 544 151.50 1.692 544 151.19 1.689 543 149.13 1.666 583 144.69 1.616 647 142.38 1.590 574 136.31 1.522 476
in D2O
KBr disc
nujol mull
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