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MS-NW-5626 p-methoxybenzenethiol C7H8OS (Mass of molecular ion: 140)
Source Temperature: 270 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 1.3 27.0 1.0 28.0 1.0 38.0 1.9 39.0 3.6 45.0 8.0 50.0 2.5 51.0 2.3 52.0 1.1 53.0 7.4 58.0 1.1 62.0 1.8 63.0 4.5 64.0 2.1 65.0 3.8 66.0 1.4 69.0 7.5 70.0 5.5 71.0 2.2 74.0 1.0 77.0 2.8 78.0 1.1 79.0 1.4 82.0 1.1 92.0 1.4 94.0 1.2 95.0 4.1 96.0 5.8 97.0 25.9 98.0 2.5 99.0 1.3 107.0 1.1 108.0 1.6 109.0 3.1 110.0 2.5 111.0 1.0 124.0 3.8 125.0 60.4 126.0 4.9 127.0 3.2 139.0 11.0 140.0 100.0 141.0 9.3 142.0 5.2 246.0 1.4
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H8 O S 0.04 ml : 0.5 ml CDCl3 p-methoxybenzenethiol Assign. Shift(ppm)
A 7.25 B 6.79 C 3.760 D 3.34
Hz ppm Int.
654.38 7.307 108 653.81 7.301 118 652.13 7.282 49 651.56 7.276 37 647.75 7.233 43 647.19 7.227 41 645.44 7.207 188 644.88 7.201 147 614.69 6.864 25 611.75 6.831 206 609.44 6.805 53 605.06 6.756 56 602.88 6.732 130 336.75 3.761 1000 299.50 3.345 165
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