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网站主页CAS数据库列表 69-09-0更多图谱盐酸氯丙嗪(69-09-0)质谱(MS)

盐酸氯丙嗪

产品名称 盐酸氯丙嗪

CAS号69-09-0

分子式C17H20Cl2N2S

分子量355.33

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  • Mass

    MS2014-05089CW      
    2-chloro-10-(3-dimethylaminopropyl)phenothiazine hydrochloride
    C17H19ClN2S HCl     (Mass of molecular ion:    318)
    

       Source Temperature: 250 °C
       Sample Temperature:  20 °C
       Direct, 70 eV
    

          18.0       1.2
          30.0       2.1
          36.0       4.9
          38.0       1.7
          42.0       4.1
          43.0       1.5
          44.0       3.4
          45.0       1.1
          56.0       1.2
          57.0       1.7
          58.0     100.0
          59.0       4.7
          63.0       1.0
          69.0       1.7
          70.0       3.4
          71.0       2.0
          72.0       3.4
          84.0       4.0
          85.0      15.3
          86.0      37.7
          87.0       2.2
         108.0       1.0
         139.0       1.6
         151.0       1.1
         152.0       2.4
         153.0       2.0
         164.0       1.4
         166.0       1.1
         178.0       1.4
         179.0       1.3
         184.0       1.1
         188.0       1.9
         196.0       4.4
         197.0       4.4
         198.0       3.0
         200.0       1.8
         201.0       1.3
         204.0       1.0
         210.0       1.8
         211.0       2.2
         212.0       2.4
         213.0       1.9
         214.0       9.2
         215.0       2.0
         216.0       3.0
         223.0       2.0
         224.0       1.1
         225.0       1.8
         232.0      14.3
         233.0      15.5
         234.0       7.2
         235.0       5.7
         236.0       1.4
         237.0       1.5
         238.0       2.4
         239.0       1.1
         244.0       1.4
         245.0       1.0
         246.0       8.5
         247.0       7.3
         248.0       3.9
         249.0       2.6
         258.0       1.6
         259.0       1.8
         260.0       2.1
         272.0      32.5
         273.0      14.9
         274.0      14.1
         275.0       5.6
         276.0       1.4
         318.0      75.3
         319.0      14.8
         320.0      28.2
         321.0       5.4
         322.0       1.6
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C17 H19 Cl N2 S 0.036 g : 0.5 ml CDCl3
    2-chloro-10-(3-dimethylaminopropyl)phenothiazine hydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.221 B 7.178 C 7.074 D 6.996 E 6.943 F 6.94 G 6.877 J 4.051 K 3.125 L 2.679 M 2.346 J(A,B)=1.6HZ J(A,D)=7.5HZ J(A,F)=8.2HZ J(B,D)=7.7HZ J(B,F)=0.4HZ J(C,E)=8.2HZ J(D,F)=1.2HZ J(E,G)=2.1HZ

         Hz     ppm     Int.
    

       2895.02   7.244     31
       2893.43   7.240     38
       2887.57   7.226     46
       2886.84   7.224     48
       2886.11   7.222     54
       2885.38   7.220     54
       2879.52   7.206     44
       2877.93   7.202     53
       2873.54   7.191     62
       2872.31   7.188     58
       2865.84   7.171     79
       2864.62   7.168     65
       2831.91   7.086    128
       2823.73   7.066    172
       2803.71   7.016     45
       2802.49   7.013     54
       2796.26   6.997     63
       2796.02   6.997     63
       2795.04   6.994     68
       2788.57   6.978     39
       2787.35   6.975     38
       2779.66   6.956    108
       2777.59   6.951    152
       2776.12   6.947     64
       2771.48   6.935     80
       2769.41   6.930    130
       2768.07   6.927     56
       2749.51   6.880    111
       2747.44   6.875     98
       1625.12   4.067     54
       1619.02   4.052     99
       1612.92   4.036     56
       1257.20   3.146     56
       1251.22   3.131     39
       1249.39   3.127     53
       1246.95   3.121     37
       1241.33   3.107     62
       1070.92   2.680   1000
        944.82   2.365     32
        939.45   2.351     35
        937.01   2.345     38
        934.94   2.340     37
        929.08   2.325     30
    

in CDCl3



KBr disc



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