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MassMS-NW-5750 3-amino-1-ethylpiperidine C7H16N2 (Mass of molecular ion: 128)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 3.1 18.0 1.7 27.0 5.9 28.0 13.2 29.0 5.8 30.0 13.1 39.0 2.9 41.0 6.9 42.0 34.6 43.0 22.8 44.0 17.4 53.0 1.1 54.0 2.5 55.0 3.0 56.0 11.4 57.0 35.5 58.0 15.1 67.0 1.3 68.0 2.8 69.0 3.9 70.0 27.5 71.0 3.5 72.0 100.0 73.0 5.1 80.0 1.0 82.0 3.7 83.0 1.6 84.0 7.3 85.0 74.4 86.0 4.7 96.0 7.2 97.0 1.1 98.0 4.3 99.0 1.8 110.0 3.3 111.0 2.0 113.0 5.5 127.0 1.0 128.0 12.0 129.0 1.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H16 N2 0.05 ml : 0.5 ml CDCl3 3-amino-1-ethylpiperidine 
Assign. Shift(ppm)
A 2.86 B 2.71 C 2.39 D 1.935 E 1.846 F 1.71 G 1.58 J 1.56 K 1.08 L 1.072 ASSIGNED BY C-H COSY
Hz ppm Int.1153.93 2.888 64 1149.78 2.877 55 1148.07 2.873 50 1144.17 2.863 112 1141.60 2.857 95 1140.38 2.854 97 1138.31 2.849 79 1134.28 2.839 93 1130.62 2.830 62 1086.67 2.720 37 1076.05 2.693 40 969.12 2.425 82 967.04 2.420 97 961.79 2.407 242 959.84 2.402 252 954.59 2.389 254 952.64 2.384 261 947.39 2.371 104 945.56 2.366 95 773.56 1.936 43 698.24 1.748 47 694.09 1.737 83 690.92 1.729 76 689.82 1.727 69 686.52 1.718 67 685.06 1.715 64 681.76 1.706 61 680.54 1.703 85 677.25 1.695 79 676.15 1.692 82 672.97 1.684 66 644.53 1.613 55 640.63 1.603 36 637.33 1.595 54 633.42 1.585 96 630.98 1.579 68 629.39 1.575 79 626.46 1.568 103 622.44 1.558 197 620.00 1.552 195 616.46 1.543 100 612.92 1.534 62 609.01 1.524 57 435.67 1.091 516 433.23 1.085 54 428.47 1.073 1000 421.26 1.055 550
in CDCl3
liquid film
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