3-氨基-N-乙基哌啶

Mass

MS-NW-5750          
3-amino-1-ethylpiperidine
C7H16N2             (Mass of molecular ion:    128)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       3.1
      18.0       1.7
      27.0       5.9
      28.0      13.2
      29.0       5.8
      30.0      13.1
      39.0       2.9
      41.0       6.9
      42.0      34.6
      43.0      22.8
      44.0      17.4
      53.0       1.1
      54.0       2.5
      55.0       3.0
      56.0      11.4
      57.0      35.5
      58.0      15.1
      67.0       1.3
      68.0       2.8
      69.0       3.9
      70.0      27.5
      71.0       3.5
      72.0     100.0
      73.0       5.1
      80.0       1.0
      82.0       3.7
      83.0       1.6
      84.0       7.3
      85.0      74.4
      86.0       4.7
      96.0       7.2
      97.0       1.1
      98.0       4.3
      99.0       1.8
     110.0       3.3
     111.0       2.0
     113.0       5.5
     127.0       1.0
     128.0      12.0
     129.0       1.1

Assign. Shift(ppm) A 2.86 B 2.71 C 2.39 D 1.935 E 1.846 F 1.71 G 1.58 J 1.56 K 1.08 L 1.072 ASSIGNED BY C-H COSY

     Hz     ppm     Int.

   1153.93   2.888     64
   1149.78   2.877     55
   1148.07   2.873     50
   1144.17   2.863    112
   1141.60   2.857     95
   1140.38   2.854     97
   1138.31   2.849     79
   1134.28   2.839     93
   1130.62   2.830     62
   1086.67   2.720     37
   1076.05   2.693     40
    969.12   2.425     82
    967.04   2.420     97
    961.79   2.407    242
    959.84   2.402    252
    954.59   2.389    254
    952.64   2.384    261
    947.39   2.371    104
    945.56   2.366     95
    773.56   1.936     43
    698.24   1.748     47
    694.09   1.737     83
    690.92   1.729     76
    689.82   1.727     69
    686.52   1.718     67
    685.06   1.715     64
    681.76   1.706     61
    680.54   1.703     85
    677.25   1.695     79
    676.15   1.692     82
    672.97   1.684     66
    644.53   1.613     55
    640.63   1.603     36
    637.33   1.595     54
    633.42   1.585     96
    630.98   1.579     68
    629.39   1.575     79
    626.46   1.568    103
    622.44   1.558    197
    620.00   1.552    195
    616.46   1.543    100
    612.92   1.534     62
    609.01   1.524     57
    435.67   1.091    516
    433.23   1.085     54
    428.47   1.073   1000
    421.26   1.055    550