1-环己烯氧基三甲基硅烷

Mass

MS-IW-7536          
1-(trimethylsilyloxy)cyclohexene
C9H18OSi            (Mass of molecular ion:    170)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0       2.9
      28.0       1.0
      29.0       1.2
      39.0       3.3
      41.0       5.4
      42.0       2.4
      43.0       5.2
      44.0       2.9
      45.0      15.5
      46.0       1.0
      47.0       5.5
      51.0       1.2
      53.0       2.9
      55.0       5.9
      56.0       1.6
      57.0       2.4
      58.0       1.3
      59.0       7.4
      60.0       1.1
      61.0       4.4
      63.5       1.1
      66.0       1.1
      67.0       1.0
      68.0       1.5
      69.0       1.9
      70.0       5.1
      71.0       1.2
      72.0       2.3
      73.0      75.5
      74.0       6.7
      75.0     100.0
      76.0       9.4
      77.0       7.8
      77.5       1.4
      78.0       1.3
      79.0       5.6
      80.0       2.2
      81.0       3.1
      83.0       1.0
      85.0       7.1
      97.0       1.1
      98.0       2.5
      99.0       3.7
     101.0       1.3
     111.0       1.8
     113.0       1.9
     125.0       1.0
     127.0      53.0
     128.0       6.4
     129.0       2.8
     141.0       6.5
     142.0      26.1
     143.0       3.7
     144.0       1.1
     147.0       7.3
     148.0       1.1
     151.0       1.4
     155.0      69.5
     156.0       9.8
     157.0       3.2
     169.0      40.0
     170.0      74.2
     171.0      12.6
     172.0       3.4

Assign. Shift(ppm) A 4.860 B 1.99 C *1 1.651 D *1 1.509 E 0.174

     Hz     ppm     Int.

   1942.50   4.861     45
    802.49   2.008     51
    800.66   2.004     53
    799.80   2.002     56
    798.58   1.999     49
    796.26   1.993     59
    794.43   1.988     65
    793.09   1.985     60
    666.50   1.668     35
    660.89   1.654     37
    654.79   1.639     35
    607.42   1.520     37
    604.98   1.514     31
    601.93   1.507     43
    595.95   1.492     38
     73.12   0.183     70
     69.58   0.175   1000
     66.53   0.167     87
     64.82   0.163     45