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MassMS-IW-7536 1-(trimethylsilyloxy)cyclohexene C9H18OSi (Mass of molecular ion: 170)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 2.9 28.0 1.0 29.0 1.2 39.0 3.3 41.0 5.4 42.0 2.4 43.0 5.2 44.0 2.9 45.0 15.5 46.0 1.0 47.0 5.5 51.0 1.2 53.0 2.9 55.0 5.9 56.0 1.6 57.0 2.4 58.0 1.3 59.0 7.4 60.0 1.1 61.0 4.4 63.5 1.1 66.0 1.1 67.0 1.0 68.0 1.5 69.0 1.9 70.0 5.1 71.0 1.2 72.0 2.3 73.0 75.5 74.0 6.7 75.0 100.0 76.0 9.4 77.0 7.8 77.5 1.4 78.0 1.3 79.0 5.6 80.0 2.2 81.0 3.1 83.0 1.0 85.0 7.1 97.0 1.1 98.0 2.5 99.0 3.7 101.0 1.3 111.0 1.8 113.0 1.9 125.0 1.0 127.0 53.0 128.0 6.4 129.0 2.8 141.0 6.5 142.0 26.1 143.0 3.7 144.0 1.1 147.0 7.3 148.0 1.1 151.0 1.4 155.0 69.5 156.0 9.8 157.0 3.2 169.0 40.0 170.0 74.2 171.0 12.6 172.0 3.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H18 O Si 0.05 ml : 0.5 ml CDCl3 1-(trimethylsilyloxy)cyclohexene 
Assign. Shift(ppm)
A 4.860 B 1.99 C *1 1.651 D *1 1.509 E 0.174
Hz ppm Int.1942.50 4.861 45 802.49 2.008 51 800.66 2.004 53 799.80 2.002 56 798.58 1.999 49 796.26 1.993 59 794.43 1.988 65 793.09 1.985 60 666.50 1.668 35 660.89 1.654 37 654.79 1.639 35 607.42 1.520 37 604.98 1.514 31 601.93 1.507 43 595.95 1.492 38 73.12 0.183 70 69.58 0.175 1000 66.53 0.167 87 64.82 0.163 45
in CDCl3
liquid film
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