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MassMS-NW-4968 4-methyl(thiosemicarbazide) C2H7N3S (Mass of molecular ion: 105)
Source Temperature: 140 °C Sample Temperature: 100 °C Direct, 75 eV
15.0 10.2 16.0 1.1 17.0 3.5 18.0 3.7 27.0 1.2 28.0 12.0 29.0 3.3 30.0 14.1 31.0 7.7 32.0 100.0 33.0 1.0 42.0 9.8 43.0 3.1 45.0 3.9 46.0 1.2 47.0 7.2 48.0 1.0 55.0 4.2 56.0 1.3 57.0 6.2 59.0 4.9 60.0 6.4 62.0 1.9 72.0 1.5 73.0 1.8 74.0 38.9 75.0 3.8 76.0 2.1 105.0 64.3 106.0 3.1 107.0 3.2
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C2 H7 N3 S 0.041 g : 0.5 ml DMSO-d6 4-methyl(thiosemicarbazide) 
Assign. Shift(ppm)
A *1 8.55 B *1 7.81 C 4.42 D 2.898
Hz ppm Int.3416.87 8.550 243 3121.46 7.811 82 1764.53 4.416 580 1160.89 2.905 977 1156.25 2.894 1000 1149.90 2.878 52
in DMSO-d6
KBr disc
nujol mull
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