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MassMS-NW-5112 aminoacetaldehyde diethyl acetal C6H15NO2 (Mass of molecular ion: 133)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 4.7 17.0 1.2 18.0 1.2 19.0 3.6 26.0 2.4 27.0 12.1 28.0 7.9 29.0 27.4 30.0 38.1 31.0 21.0 41.0 1.8 42.0 14.3 43.0 5.4 44.0 16.9 45.0 11.3 46.0 3.2 47.0 100.0 48.0 1.2 58.0 4.7 59.0 3.6 60.0 26.3 61.0 1.4 72.0 1.1 75.0 36.0 76.0 1.3 84.0 1.5 87.0 2.7 88.0 22.3 89.0 1.5 100.0 1.3 103.0 68.6 104.0 4.2
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H15 N O2 0.04 ml : 0.5 ml CDCl3 aminoacetaldehyde diethyl acetal 
Assign. Shift(ppm)
A 4.416 B *1 3.68 C *1 3.56 D 2.778 E 1.26 F 1.226 J(B,C)=-9.3HZ J(B,F)=7.0HZ J(C,F)=6.9HZ
Hz ppm Int.400.81 4.476 67 395.63 4.418 144 390.50 4.361 76 341.56 3.814 54 339.31 3.789 58 334.44 3.735 67 332.13 3.709 173 331.31 3.700 85 327.44 3.657 42 325.00 3.629 214 324.25 3.621 191 321.94 3.595 36 317.25 3.543 183 314.81 3.516 63 310.38 3.466 70 307.88 3.438 58 251.38 2.807 114 248.81 2.779 46 246.31 2.751 112 116.56 1.302 488 112.75 1.259 190 109.56 1.224 1000 102.50 1.145 411
in CDCl3
liquid film
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