氨基乙醛缩二乙醇

Mass

MS-NW-5112          
aminoacetaldehyde diethyl acetal
C6H15NO2            (Mass of molecular ion:    133)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       4.7
      17.0       1.2
      18.0       1.2
      19.0       3.6
      26.0       2.4
      27.0      12.1
      28.0       7.9
      29.0      27.4
      30.0      38.1
      31.0      21.0
      41.0       1.8
      42.0      14.3
      43.0       5.4
      44.0      16.9
      45.0      11.3
      46.0       3.2
      47.0     100.0
      48.0       1.2
      58.0       4.7
      59.0       3.6
      60.0      26.3
      61.0       1.4
      72.0       1.1
      75.0      36.0
      76.0       1.3
      84.0       1.5
      87.0       2.7
      88.0      22.3
      89.0       1.5
     100.0       1.3
     103.0      68.6
     104.0       4.2

Assign. Shift(ppm) A 4.416 B *1 3.68 C *1 3.56 D 2.778 E 1.26 F 1.226 J(B,C)=-9.3HZ J(B,F)=7.0HZ J(C,F)=6.9HZ

     Hz     ppm     Int.

    400.81   4.476     67
    395.63   4.418    144
    390.50   4.361     76
    341.56   3.814     54
    339.31   3.789     58
    334.44   3.735     67
    332.13   3.709    173
    331.31   3.700     85
    327.44   3.657     42
    325.00   3.629    214
    324.25   3.621    191
    321.94   3.595     36
    317.25   3.543    183
    314.81   3.516     63
    310.38   3.466     70
    307.88   3.438     58
    251.38   2.807    114
    248.81   2.779     46
    246.31   2.751    112
    116.56   1.302    488
    112.75   1.259    190
    109.56   1.224   1000
    102.50   1.145    411