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网站主页CAS数据库列表 64168-11-2更多图谱4,4'-三亚甲基双(1-甲基哌啶)(64168-11-2)红外图谱(IR1)

4,4'-三亚甲基双(1-甲基哌啶)

产品名称 4,4'-三亚甲基双(1-甲基哌啶)

CAS号64168-11-2

分子式C15H30N2

分子量238.41


  • Mass

    MS-IW-1270          
    4,4'-trimethylenebis(1-methylpiperidine)
    C15H30N2            (Mass of molecular ion:    238)
    

       Source Temperature: 230 °C
       Sample Temperature: 160 °C
       Reservoir, 75 eV
    

          27.0       1.0
          29.0       2.6
          30.0       1.2
          39.0       1.4
          41.0       5.9
          42.0      15.5
          43.0      13.0
          44.0      30.0
          53.0       1.4
          55.0       9.8
          56.0       2.4
          57.0       7.3
          58.0      27.2
          59.0       1.5
          67.0       2.0
          68.0       1.3
          69.0       1.6
          70.0      34.8
          71.0      10.4
          72.0       3.6
          79.0       1.0
          81.0       2.0
          82.0       2.4
          83.0       1.3
          84.0       2.1
          94.0       2.1
          96.0      52.2
          97.0       5.5
          98.0      24.0
          99.0      14.0
         100.0       1.0
         110.0       4.1
         112.0      21.0
         113.0       5.0
         118.0       4.1
         122.0       1.3
         124.0       1.3
         126.0      20.7
         127.0       6.2
         138.0       2.2
         140.0      32.0
         141.0       4.3
         152.0       1.1
         154.0       1.4
         166.0       4.6
         167.0       1.5
         168.0      13.3
         169.0       1.8
         178.0       1.3
         180.0       3.8
         181.0       5.9
         182.0       4.6
         192.0       2.2
         194.0      11.2
         195.0       7.0
         196.0       1.5
         207.0       1.3
         208.0       5.2
         209.0       6.0
         210.0       2.5
         221.0       1.0
         223.0     100.0
         224.0      16.1
         225.0       1.2
         236.0       1.9
         237.0      34.7
         238.0      59.0
         239.0      10.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C15 H30 N2 0.05 ml : 0.5 ml CDCl3
    4,4'-trimethylenebis(1-methylpiperidine)
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.825 B 2.251 C 1.882 D 1.661 E 1.28 F 1.22 to 1.20

         Hz     ppm     Int.
    

       1135.50   2.842    130
       1123.66   2.812    136
        899.54   2.251   1000
        763.31   1.910     89
        751.95   1.882    154
        740.48   1.853     82
        669.80   1.676     90
        667.60   1.671     95
        657.23   1.645    130
        520.02   1.302     42
        512.94   1.284     61
        511.11   1.279     58
        502.44   1.258     72
        498.78   1.249     78
        490.48   1.228    142
        486.08   1.217    198
        478.76   1.198    256
        471.44   1.180     90
    

in CDCl3



liquid film