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N-甲基哌啶

产品名称 N-甲基哌啶

CAS号626-67-5

分子式C6H13N

分子量99.17

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  • Mass

    MS-NW-3134          
    1-methylpiperidine
    C6H13N              (Mass of molecular ion:     99)
    

       Source Temperature: 280 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          15.0       4.1
          27.0       5.6
          28.0       2.8
          29.0       2.8
          30.0       1.9
          39.0       5.1
          41.0       7.3
          42.0      29.1
          43.0      46.4
          44.0       9.1
          53.0       1.3
          54.0       1.6
          55.0       6.0
          56.0       2.5
          57.0       8.6
          58.0      13.0
          68.0       1.6
          70.0      16.1
          71.0       9.5
          82.0       1.2
          84.0       7.7
          96.0       2.0
          98.0     100.0
          99.0      43.2
         100.0       2.7
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C6 H13 N 0.05 ml : 0.5 ml CDCl3
    1-methylpiperidine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.33 B 2.234 C 1.586 D 1.41

         Hz     ppm     Int.
    

        929.69   2.327     94
        893.07   2.235   1000
        646.00   1.617    101
        640.14   1.602    239
        634.52   1.588    306
        628.78   1.574    284
        623.29   1.560    114
        563.23   1.410     73
    


  • 1H NMR 89.56 MHz
    C6 H13 N 0.05 ml : 0.5 ml CDCl3
    1-methylpiperidine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.33 B 2.232 C 1.59 to 1.48

         Hz     ppm     Int.
    

        213.38   2.383     53
        212.94   2.378     53
        208.88   2.333     89
        203.31   2.271     85
        200.00   2.234   1000
        197.31   2.204     32
        147.56   1.648     37
        143.06   1.598     58
        141.56   1.581     62
        137.06   1.531     62
        133.63   1.493     76
        133.06   1.486     73
        132.94   1.485     73
        130.00   1.452     40
        128.25   1.433     29
        126.06   1.408     22
    

in CDCl3



liquid film